4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-

Base Information

Chemical Name:4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-
CAS No.:935864-45-2
Molecular Formula:C₂₄H₂₂N₂O₄
Molecular Weight:402.45
Hs Code.:
Mol file:935864-45-2.mol

Synonyms:4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-

Suppliers and Price of 4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-

Chemical Property:

Melting Point:219-221 °C
Boiling Point:621.0±55.0 °C (760 mmHg)
PSA：80.42000
Density:1.241±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:4.06190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo-

There total 4 articles about 4-AcridinecarboxaMide, 9,10-dihydro-6-Methoxy-N-[2-(4-Methoxyphenyl)ethyl]-9-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21971-21-1
2-chloro-4-methoxybenzoic acid

: 935864-45-2
6-methoxy-9-oxo-9,10-dihydro-acridine-4-carboxylic acid [2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / copper / 3-methyl-butan-1-ol / 10 h / 160 °C

2: H₃PO₄; P₂O₅ / 3 h / 110 °C

3: N,N'-dicyclohexylcarbodiimide; triethylamine

With phosphoric acid; phosphorus pentoxide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; copper; In i-Amyl alcohol;
DOI:10.1016/j.bmc.2007.02.017

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 935864-45-2
6-methoxy-9-oxo-9,10-dihydro-acridine-4-carboxylic acid [2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / copper / 3-methyl-butan-1-ol / 10 h / 160 °C

2: H₃PO₄; P₂O₅ / 3 h / 110 °C

3: N,N'-dicyclohexylcarbodiimide; triethylamine

With phosphoric acid; phosphorus pentoxide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; copper; In i-Amyl alcohol;
DOI:10.1016/j.bmc.2007.02.017

Reference yield:

: 84126-73-8
2-<(2-carboxyphenyl)amino>-4-methoxybenzoic acid

: 935864-45-2
6-methoxy-9-oxo-9,10-dihydro-acridine-4-carboxylic acid [2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: H₃PO₄; P₂O₅ / 3 h / 110 °C

2: N,N'-dicyclohexylcarbodiimide; triethylamine

With phosphoric acid; phosphorus pentoxide; triethylamine; dicyclohexyl-carbodiimide;
DOI:10.1016/j.bmc.2007.02.017