3-(Benzyloxy)-4-nitrobenzenecarboxylic acid

Base Information

Chemical Name:3-(Benzyloxy)-4-nitrobenzenecarboxylic acid
CAS No.:14617-29-9
Molecular Formula:C14H11NO5
Molecular Weight:273.245
Hs Code.:2918990090
Mol file:14617-29-9.mol

Synonyms:3-(Benzyloxy)-4-nitrobenzenecarboxylic acid

Suppliers and Price of 3-(Benzyloxy)-4-nitrobenzenecarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
3-(Benzyloxy)-4-nitrobenzenecarboxylic acid
500 mg
$ 240.00

SynQuest Laboratories
3-(Benzyloxy)-4-nitrobenzenecarboxylic acid
1 g
$ 320.00

Matrix Scientific
3-(Benzyloxy)-4-nitrobenzenecarboxylic acid
500mg
$ 262.00

Matrix Scientific
3-(Benzyloxy)-4-nitrobenzenecarboxylic acid
1g
$ 328.00

Crysdot
3-(Benzyloxy)-4-nitrobenzoicacid 95+%
5g
$ 609.00

AK Scientific
3-(Benzyloxy)-4-nitrobenzenecarboxylicacid
1g
$ 492.00

Acrotein
3-(Benzyloxy)-4-nitrobenzoicacid 97%
0.25g
$ 133.33

Total 5 raw suppliers

Chemical Property of 3-(Benzyloxy)-4-nitrobenzenecarboxylic acid

Chemical Property:

PSA：92.35000
LogP:3.39520

Purity/Quality:

98%min ^*data from raw suppliers

3-(Benzyloxy)-4-nitrobenzenecarboxylic acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(Benzyloxy)-4-nitrobenzenecarboxylic acid

There total 4 articles about 3-(Benzyloxy)-4-nitrobenzenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 209528-69-8
methyl 3-(benzyloxy)-4-nitrobenzoate

: 14617-29-9
4-nitro-3-phenylmethoxybenzoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; at 60 ℃; for 3h;

Reference yield: 85.0%

: 403-21-4
3-fluoro-4-nitrobenzoic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 14617-29-9
4-nitro-3-phenylmethoxybenzoic acid

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.25h; Inert atmosphere;

3-fluoro-4-nitrobenzoic acid; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; for 2.08333h; Inert atmosphere;

Reference yield:

: 713-52-0
methyl 3-hydroxy-4-nitrobenzoate

: 14617-29-9
4-nitro-3-phenylmethoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; methanol; water / 12 h / 20 °C

2.2: Acidic conditions

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.11.078