Technology Process of Methyl quinoxaline-5-carboxylate
There total 7 articles about Methyl quinoxaline-5-carboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
water;
for 0.75h;
Reflux;
Inert atmosphere;
DOI:10.1021/jo400949p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid / 2.5 h / 90 °C / Inert atmosphere
2: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / Inert atmosphere
3: hydrogenchloride / water / 12 h / Reflux; Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / methanol / 8 h / Inert atmosphere
5: water / 0.75 h / Reflux; Inert atmosphere
With
hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hydroxide;
In
methanol; water;
DOI:10.1021/jo400949p
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydroxylamine hydrochloride; sodium sulfate; hydrogenchloride / water / 65 °C / Inert atmosphere
2: sulfuric acid / 2.5 h / 90 °C / Inert atmosphere
3: sodium hydroxide; dihydrogen peroxide / water / 0 - 20 °C / Inert atmosphere
4: hydrogenchloride / water / 12 h / Reflux; Inert atmosphere
5: palladium 10% on activated carbon; hydrogen / methanol / 8 h / Inert atmosphere
6: water / 0.75 h / Reflux; Inert atmosphere
With
hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; dihydrogen peroxide; sodium sulfate; sodium hydroxide;
In
methanol; water;
DOI:10.1021/jo400949p
