8-Phenylnaphthalene-2-carboxaldehyde

Base Information

Chemical Name:8-Phenylnaphthalene-2-carboxaldehyde
CAS No.:56432-19-0
Molecular Formula:C₁₇H₁₂O
Molecular Weight:232.282
Hs Code.:
DSSTox Substance ID:DTXSID20480784
Wikidata:Q82315855
Mol file:56432-19-0.mol

Synonyms:8-Phenylnaphthalene-2-carboxaldehyde;56432-19-0;SCHEMBL7720416;DTXSID20480784;FT-0763110

Suppliers and Price of 8-Phenylnaphthalene-2-carboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 8-Phenylnaphthalene-2-carboxaldehyde

Chemical Property:

PSA：17.07000
LogP:4.31930
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:232.088815002
Heavy Atom Count:18
Complexity:279

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=CC3=C2C=C(C=C3)C=O

Technology Process of 8-Phenylnaphthalene-2-carboxaldehyde

There total 7 articles about 8-Phenylnaphthalene-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₄O

: 56432-19-0
8-phenyl-2-naphthaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1002/cmdc.201500150

Reference yield:

: 135-19-3
β-naphthol

: 56432-19-0
8-phenyl-2-naphthaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dichloromethane / 16 h / 25 °C / Inert atmosphere

2: [bis(pyridine)iodine]⁺ tetrafluoroborate; trifluorormethanesulfonic acid / dichloromethane / 22 h / 25 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 110 °C / Inert atmosphere; Microwave irradiation

4: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 2 h / 70 °C

5: diisobutylaluminium hydride / hexane; tetrahydrofuran / 4 h / -78 °C / Inert atmosphere

6: manganese(IV) oxide / dichloromethane / 3 h / 25 °C / Inert atmosphere

With pyridine; manganese(IV) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; diisobutylaluminium hydride; sodium carbonate; [bis(pyridine)iodine]⁺ tetrafluoroborate; triethylamine; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; 3: |Suzuki Coupling;
DOI:10.1002/cmdc.201500150

Reference yield:

: 3857-83-8
2-naphthyl triflate

: 56432-19-0
8-phenyl-2-naphthaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: [bis(pyridine)iodine]⁺ tetrafluoroborate; trifluorormethanesulfonic acid / dichloromethane / 22 h / 25 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / 110 °C / Inert atmosphere; Microwave irradiation

3: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 2 h / 70 °C

4: diisobutylaluminium hydride / hexane; tetrahydrofuran / 4 h / -78 °C / Inert atmosphere

5: manganese(IV) oxide / dichloromethane / 3 h / 25 °C / Inert atmosphere

With manganese(IV) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; diisobutylaluminium hydride; sodium carbonate; [bis(pyridine)iodine]⁺ tetrafluoroborate; triethylamine; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; 2: |Suzuki Coupling;
DOI:10.1002/cmdc.201500150