BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-

Base Information

Chemical Name:BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-
CAS No.:869497-70-1
Molecular Formula:C19H19BrO6
Molecular Weight:423.257
Hs Code.:
Mol file:869497-70-1.mol

Synonyms:BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-

Suppliers and Price of BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

American Custom Chemicals Corporation
(ALPHAE)-3-BROMO-4-METHOXY-ALPHA-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]BENZENEACETIC ACID 95.00%
5MG
$ 504.23

Total 0 raw suppliers

Chemical Property of BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-

Chemical Property:

PSA：74.22000
LogP:4.10870

Purity/Quality:: (ALPHAE)-3-BROMO-4-METHOXY-ALPHA-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]BENZENEACETIC ACID 95.00% ^*data from reagent suppliers

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Technology Process of BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)-

There total 1 articles about BENZENEACETIC ACID, 3-BROMO-4-METHOXY-A-[(3,4,5-TRIMETHOXYPHENYL)METHYLENE]-, (AE)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 774-81-2
(3-bromo-4-methoxy-phenyl)-acetic acid

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 869497-70-1
(E)-2-(3'-bromo-4'-methoxyphenyl)-3-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: (Z)-2-(3'-bromo-4'-methoxyphenyl)-3-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Guidance literature:: With acetic anhydride; triethylamine; at 130 ℃; for 5h;
DOI:10.3184/030823408X324751

Reference yield: 91.1%

: 869497-70-1
(E)-2-(3'-bromo-4'-methoxyphenyl)-3-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: 942912-87-0
(E)-2-(3-amino-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)acrylic acid

Guidance literature:: With ammonium hydroxide; copper(l) iodide; at 80 ℃; for 48h; Sealed tube;
DOI:10.1039/c3ob41588k

Reference yield: 86.0%

: 869497-70-1
(E)-2-(3'-bromo-4'-methoxyphenyl)-3-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: Z-1-(3',4',5'-trimethoxyphenyl)-2-(3''-bromo-4''-methoxyphenyl)ethene

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; at 180 - 190 ℃; Microwave irradiation; Inert atmosphere; Green chemistry;
DOI:10.1039/c3ob41588k