Phenacyldithiocarbamic acid methyl ester

Base Information

• Chemical Name: Phenacyldithiocarbamic acid methyl ester
• CAS No.: 20184-96-7
• Molecular Formula: C10H11NOS2
• Molecular Weight: 225.335
• Mol file: 20184-96-7.mol

Synonyms:Phenacyldithiocarbamic acid methyl ester

Chemical Property of Phenacyldithiocarbamic acid methyl ester

Chemical Property:

• PSA: 77.70000
• LogP: 2.40650

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenacyldithiocarbamic acid methyl ester

There total 2 articles about Phenacyldithiocarbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

carbon disulfide (75-15-0,12122-00-8) + benzamide (55-21-0,27208-38-4) + dimethyl sulfate (77-78-1) → dimethyl N-benzoyldithiocarbonimidate (24786-18-3) + N-Benzoylamino-dithiokohlensaeuremethylester (21406-30-4) + Methyl N-benzoyl-N-methyl-carbamodithioate (20184-96-7) + N,N-dimethylbenzamide (611-74-5)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1002/hc.10173

Reference yield:

→ Methyl N-benzoyl-N-methyl-carbamodithioate (20184-96-7)

Guidance literature:

aus IIa durch Pyrolyse;

DOI:10.1246/bcsj.44.841

upstream raw materials:

carbon disulfide

benzamide

dimethyl sulfate

Refernces