2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE

Base Information

Chemical Name:2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE
CAS No.:85160-82-3
Molecular Formula:C₉H₈N₂O₄
Molecular Weight:208.174
Hs Code.:2934999090
Mol file:85160-82-3.mol

Synonyms:2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE;2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one, 97%

Suppliers and Price of 2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one
25mg
$ 90.00

SynQuest Laboratories
2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one
1 g
$ 176.00

Sigma-Aldrich
2-Methyl-7-nitro-2H-benzo[b][1,4]oxazin-3(4H)-one
1g
$ 388.00

Matrix Scientific
2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one
1g
$ 215.00

Crysdot
2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one 95+%
25g
$ 564.00

Chemenu
2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one 95%
25g
$ 533.00

American Custom Chemicals Corporation
2-METHYL-7-NITRO-2H-BENZO[B]-[1,4]-OXAZIN-3-(4H)-ONE 95.00%
5MG
$ 498.26

Alichem
2-Methyl-7-nitro-2,4-dihydro-1,4-benzoxazin-3-one
10g
$ 538.02

Alichem
2-Methyl-7-nitro-2,4-dihydro-1,4-benzoxazin-3-one
5g
$ 373.32

AK Scientific
2-Methyl-7-nitro-2,4-dihydro-1,4-benzoxazin-3-one
5g
$ 291.00

Total 8 raw suppliers

Chemical Property of 2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE

Chemical Property:

PSA：84.15000
LogP:1.97540

Purity/Quality:

99%, ^*data from raw suppliers

2-Methyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE

There total 5 articles about 2-METHYL-7-NITRO-2H-BENZO[B][1,4]OXAZIN-3(4H)-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 535-11-5,41978-69-2
Ethyl 2-bromopropionate

: 121-88-0
5-Nitro-2-aminophenol

: 85160-82-3
2-methyl-7-nitro-2-hydro-1,4-benzomorpholin-3-(4-hydro)-one

Guidance literature:: With potassium fluoride; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 6h;
DOI:10.1055/s-1982-30037

Reference yield: 77.0%

: 7623-09-8
2-chloropropionyl chloride

: 121-88-0
5-Nitro-2-aminophenol

: 85160-82-3
2-methyl-7-nitro-2-hydro-1,4-benzomorpholin-3-(4-hydro)-one

Guidance literature:: With sodium hydrogencarbonate; In water; Heating;
DOI:10.1021/jm061329j

Reference yield: 75.0%

: 5445-17-0
Methyl 2-bromopropionate

: 121-88-0
5-Nitro-2-aminophenol

: 85160-82-3
2-methyl-7-nitro-2-hydro-1,4-benzomorpholin-3-(4-hydro)-one

Guidance literature:: Methyl 2-bromopropionate; With potassium fluoride; In N,N-dimethyl-formamide; at 10 - 35 ℃; for 0.25h;

5-Nitro-2-aminophenol; In N,N-dimethyl-formamide; at 10 - 60 ℃; for 20h;