2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)

Base Information

Chemical Name:2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)
CAS No.:287184-98-9
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:
Mol file:287184-98-9.mol

Synonyms:2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)

Suppliers and Price of 2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)

Chemical Property:

PSA：46.61000
LogP:1.81240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI)

There total 5 articles about 2-Oxazolidinone,5-ethyl-3-(1-oxo-2-propenyl)-4-(2-propenyl)-,(4S,5S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 625-36-5
2-chloropropionyl chloride

: 287184-94-5
(4S,5S)-4-allyl-5-ethyl-oxazolidin-2-one

: 287184-98-9
(4S,5S)-3-Acryloyl-4-allyl-5-ethyl-oxazolidin-2-one

Guidance literature:: 2-chloropropionyl chloride; (4S,5S)-4-allyl-5-ethyl-oxazolidin-2-one; With ethylmagnesium bromide; In tetrahydrofuran;

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)00580-3

Reference yield:

: 287184-92-3
(3S,6S,7S)-6-ethyl-3-phenyltetrahydro-1,5-dioxa-3a-aza-pentalen-4-one

: 287184-98-9
(4S,5S)-3-Acryloyl-4-allyl-5-ethyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: 71 percent / TiCl₄ / CH₂Cl₂ / -78 °C

2.1: 93 percent / Na; NH₃ / ethanol; tetrahydrofuran

3.1: EtMgBr / tetrahydrofuran

3.2: 67 percent / Et₃N / CH₂Cl₂

With ethylmagnesium bromide; ammonia; sodium; titanium tetrachloride; In tetrahydrofuran; ethanol; dichloromethane; 1.1: Ring cleavage / 2.1: Reduction / 3.1: Acylation / 3.2: Unknown;
DOI:10.1016/S0040-4039(00)00580-3

Reference yield:

: 287184-93-4
(4S,5S,6S)-4-allyl-5-ethyl-3-(2-hydroxy-1-phenylethyl)-oxazolidin-2-one

: 287184-98-9
(4S,5S)-3-Acryloyl-4-allyl-5-ethyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 93 percent / Na; NH₃ / ethanol; tetrahydrofuran

2.1: EtMgBr / tetrahydrofuran

2.2: 67 percent / Et₃N / CH₂Cl₂

With ethylmagnesium bromide; ammonia; sodium; In tetrahydrofuran; ethanol; 1.1: Reduction / 2.1: Acylation / 2.2: Unknown;
DOI:10.1016/S0040-4039(00)00580-3