4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)

Base Information

Chemical Name:4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)
CAS No.:258333-49-2
Molecular Formula:C10H14N2
Molecular Weight:162.23
Hs Code.:
Mol file:258333-49-2.mol

Synonyms:4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)

Suppliers and Price of 4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)

Chemical Property:

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Technology Process of 4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI)

There total 4 articles about 4,7-Iminocyclohepta[b]pyrrole,1,4,5,6,7,8-hexahydro-9-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 258333-51-6
5-methyl-1-vinyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine

: 258333-49-2
5-methyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine

Guidance literature:: 5-methyl-1-vinyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine; With mercury(II) diacetate; In tetrahydrofuran; for 2h; Heating;

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; at 60 - 70 ℃; for 2h;
DOI:10.1007/BF02324648

Reference yield:

: 1515-26-0,14587-46-3
tropinone oxime

: 74-86-2,25067-58-7
acetylene

: 258333-49-2
5-methyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine

: 258333-51-6
5-methyl-1-vinyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 95 - 100 ℃;
DOI:10.1007/BF02324648

Reference yield:

: 532-24-1
tropinone

: 258333-49-2
5-methyl-4,5,6,7-tetrahydro-4,6-ethanopyrrolo[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / hydroxylamine hydrochloride; sodium acetate trihydrate / ethanol / 4.5 h / Heating

2: KOH / dimethylsulfoxide / 95 - 100 °C

With potassium hydroxide; hydroxylamine hydrochloride; sodium acetate; In ethanol; dimethyl sulfoxide; 1: Condensation / 2: Cyclization;
DOI:10.1007/BF02324648