5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole

Base Information

Chemical Name:5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole
CAS No.:1211-65-0
Molecular Formula:C11H11 N O4
Molecular Weight:221.213
Hs Code.:
Mol file:1211-65-0.mol

Synonyms:1,3-Benzodioxole,5-(2-nitro-1-butenyl)- (9CI); Benzene,1,2-(methylenedioxy)-4-(2-nitro-1-butenyl)- (7CI,8CI); NSC 14007

Suppliers and Price of 5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole

Chemical Property:

Vapor Pressure:0.000101mmHg at 25°C
Boiling Point:348.5°Cat760mmHg
Flash Point:159.6°C
Density:1.296g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole

There total 1 articles about 5-(2-nitrobut-1-en-1-yl)-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 108-03-2
1-Nitropropane

: 1211-65-0
1-(3,4-Methylenedioxyphenyl)-2-nitro-1-butene

: 4421-09-4
piperonylonitrile

Guidance literature:: isobutylamine; In acetic acid; at 50 ℃; for 2h; under 7500600 Torr;
DOI:10.1007/BF00960337

Reference yield:

: 1211-65-0
1-(3,4-Methylenedioxyphenyl)-2-nitro-1-butene

: 107447-03-0
1-(3,4-methylenedioxyphenyl)-2-butanamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;
DOI:10.1007/BF00960337

Reference yield:

: 1211-65-0
1-(3,4-Methylenedioxyphenyl)-2-nitro-1-butene

: 128767-12-4
1-(3,4-Methylenedioxyphenyl)-2-methylaminobutane hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 19.16 g / LiAlH₄ / tetrahydrofuran / 1 h / Heating

2: 7 h / Heating

3: LiAlH₄, HCl / tetrahydrofuran / 1 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1007/BF00960337