1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose

Base Information

Chemical Name:1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose
CAS No.:4933-77-1
Molecular Formula:C12H20O6
Molecular Weight:258.271
Hs Code.:
Mol file:4933-77-1.mol

Synonyms:1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose;(3aR,5S,5aR,8aS,8bR)-2,2,7,7-tetramethyltetrahydro-5H-bis([1,3]dioxolo)[4,5-b:4',5'-d]pyran-5-carbaldehyde

Suppliers and Price of 1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1,2:3,4-Di-o-isopropylidene-alpha-D-galacto-hexadialdo-1,5-pyranose 97%
1g
$ 355.00

Total 4 raw suppliers

Chemical Property of 1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose

Chemical Property:

PSA：66.38000
LogP:0.37520
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1,2:3,4-Di-o-isopropylidene-alpha-D-galacto-hexadialdo-1,5-pyranose 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose

There total 17 articles about 1,2:3,4-Di-O-isopropylidene-α-D-galacto-hexadialdo-1,5-pyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 4933-77-1
(3aR,5S,5aR,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-carbaldehyde

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; for 4h; Heating;
DOI:10.1021/jo0602017

Reference yield: 83.0%

: 1010075-67-8
C₁₅H₂₄O₅S₂

: 4933-77-1
(3aR,5S,5aR,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-carbaldehyde

Guidance literature:: With Amberlyst A (trifluoroacetoxy)iodate(I) form; In water; acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1021/jo7025146

Reference yield: 71.0%

: 108678-44-0
tert-butyldimethyl(2,2,7,7-tetramethyltetrahydrobis[1,3]dioxolo[5,4-b:4',5'-d]pyran-5-ylmethoxy)silane

: 4933-77-1
(3aR,5S,5aR,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-carbaldehyde

Guidance literature:: tert-butyldimethyl(2,2,7,7-tetramethyltetrahydrobis[1,3]dioxolo[5,4-b:4',5'-d]pyran-5-ylmethoxy)silane; With bismuth(lll) trifluoromethanesulfonate; water; In acetonitrile; for 1.5h;

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1055/s-0030-1260980