(13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate

Base Information

Chemical Name:(13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate
CAS No.:29944-26-1
Molecular Formula:C22H27NO6
Molecular Weight:401.45288
Hs Code.:
Mol file:29944-26-1.mol

Synonyms:(13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate;9α-Acetoxyindolinocodeinone dimethyl acetal

Suppliers and Price of (13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate

Chemical Property:

Melting Point:123 - 124.5 °C
PSA：66.46000
LogP:1.75290

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate

There total 7 articles about (13β,14β)-7,8-Didehydro-4,5α-epoxy-3,6,6-trimethoxy-17-methylhasubanan-9α-ol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115-37-7
thebaine

: 29944-26-1
ent-9β-acetoxy-4,5β-epoxy-3,6,6-trimethoxy-17-methyl-hasuban-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂

2: methanol

With bromine; In methanol;
DOI:10.1039/P19730000316

Reference yield:

: 4599-09-1
14-bromo-4,5α-epoxy-3,6,6-trimethoxy-17-methyl-morphin-7-ene

: 29944-26-1
ent-9β-acetoxy-4,5β-epoxy-3,6,6-trimethoxy-17-methyl-hasuban-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: AgClO₄ / benzene

2: dimethylformamide; H₂O

With silver perchlorate; In water; N,N-dimethyl-formamide; benzene;
DOI:10.1039/P19730000363

Reference yield:

: 29944-25-0
4,5α-epoxy-7β-iodo-3,6,6-trimethoxy-17-methyl-morphin-8(14)-ene

: 29944-26-1
ent-9β-acetoxy-4,5β-epoxy-3,6,6-trimethoxy-17-methyl-hasuban-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: AgClO₄ / benzene

2: dimethylformamide; H₂O

With silver perchlorate; In water; N,N-dimethyl-formamide; benzene;
DOI:10.1039/P19730000363