3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

Base Information

Chemical Name:3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
CAS No.:1233200-57-1
Molecular Formula:C24H17Br
Molecular Weight:385.303
Hs Code.:
Mol file:1233200-57-1.mol

Synonyms:3-Bromo-5'-phenyl-1,1':3',1''-terphenyl;3',5'-Diphenyl-3-broMobiphenyl;1-(3-BROMOPHENYL)-3,5-DIPHENYLBENZENE

Suppliers and Price of 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-5''-phenyl-1,1'':3'',1''''-terphenyl
50mg
$ 60.00

TCI Chemical
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl >98.0%(GC)
1g
$ 42.00

TCI Chemical
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl >98.0%(GC)
5g
$ 207.00

Crysdot
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
100g
$ 854.00

Crysdot
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
25g
$ 335.00

Arctom
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
100g
$ 837.00

Arctom
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
25g
$ 335.00

Arctom
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
5g
$ 112.00

Arctom
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
1g
$ 38.00

Arctom
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl 97%
250mg
$ 16.00

Total 23 raw suppliers

Chemical Property of 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

Chemical Property:

Melting Point:112.0 to 116.0 °C
Boiling Point:497.8±14.0 °C(Predicted)
PSA：0.00000
Density:1.278±0.06 g/cm3(Predicted)
LogP:7.45010
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

3-Bromo-5''-phenyl-1,1'':3'',1''''-terphenyl ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

There total 5 articles about 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 591-18-4
1-Bromo-3-iodobenzene

: 1036378-83-2
2-([1,1':3′,1''-terphenyl]-5'-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1233200-57-1
3-bromo-5′-phenyl-1,1′:3′,1″-terphenyl

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; at 80 ℃; for 12h; Inert atmosphere;

Reference yield: 71.0%

: 14473-91-7,20595-41-9,32862-97-8
3-bromocinnamic acid

: 35491-57-7
(E,Z)-2-benzoyl-3-phenylbut-2-enenitrile

: 1233200-57-1
3-bromo-5′-phenyl-1,1′:3′,1″-terphenyl

Guidance literature:: 3-bromocinnamic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h; Schlenk technique; Inert atmosphere;

(E,Z)-2-benzoyl-3-phenylbut-2-enenitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.8b01740

Reference yield:

: 103068-20-8
1-bromo-3,5-diphenylbenzene

: 1233200-57-1
3-bromo-5′-phenyl-1,1′:3′,1″-terphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 10 h / 150 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;