3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo

Base Information

Chemical Name:3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo
CAS No.:444289-55-8
Molecular Formula:C₃₄H₄₅B₂NO₄
Molecular Weight:553.358
Hs Code.:

Synonyms:3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo

Suppliers and Price of 3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 6 raw suppliers

Chemical Property of 3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo

There total 8 articles about 3-((4-((4-butylphenyl)(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)phenyl)(methyl)bo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 276690-04-1
4-bromo-N-(4-bromophenyl)-N-(4-butylphenyl)aniline

: 444289-55-8
4-butyl-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;
DOI:10.1039/c5tc01794g

Reference yield:

: 152270-84-3
N-(4-n-butylphenyl)-N-phenylbenzenamine

: 444289-55-8
4-butyl-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: 65.5 percent / CuBr₂; Al₂O₃ / CCl₄ / 2 h / 60 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: trimethyl borate / tetrahydrofuran; hexane / -78 - 20 °C

2.3: aq. HCl / tetrahydrofuran; hexane

3.1: 2.18 g / benzene / Heating

With aluminum oxide; n-butyllithium; copper(ll) bromide; In tetrahydrofuran; tetrachloromethane; hexane; benzene;
DOI:10.1021/ma051842r

Reference yield:

: 276690-04-1
4-bromo-N-(4-bromophenyl)-N-(4-butylphenyl)aniline

: 444289-55-8
4-butyl-N,N-bis(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: trimethyl borate / tetrahydrofuran; hexane / -78 - 20 °C

1.3: aq. HCl / tetrahydrofuran; hexane

2.1: 2.18 g / benzene / Heating

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/ma051842r