Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-

Base Information

Chemical Name:Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-
CAS No.:1403677-99-5
Molecular Formula:C27H21N3
Molecular Weight:387.484
Hs Code.:

Synonyms:Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-;(2-(4-(azidoMethyl)phenyl)ethene-1,1,2-triyl)tribenzene

Suppliers and Price of Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 15 raw suppliers

Chemical Property of Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-

Chemical Property:

PSA：49.75000
LogP:6.95706

Purity/Quality:: ≥99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)-

There total 7 articles about Benzene, 1-(azidoMethyl)-4-(1,2,2-triphenylethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1361969-01-8
(2-(4-(bromomethyl)phenyl)ethene-1,1,2-triyl)tribenzene

: 1403677-99-5
(2-(4-(azidomethyl)phenyl)ethene-1,1,2-triyl)tribenzene

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja3064588

Reference yield:

: 125847-08-7
1-(4-methylphenyl)-1,2,2-triphenylethanol

: 1403677-99-5
(2-(4-(azidomethyl)phenyl)ethene-1,1,2-triyl)tribenzene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux

3: sodium azide / dimethyl sulfoxide / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium azide; toluene-4-sulfonic acid; dibenzoyl peroxide; In tetrachloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/ja3064588

Reference yield:

: 70592-06-2
1,1,2-triphenyl-2-(p-methylphenyl)ethylene

: 1403677-99-5
(2-(4-(azidomethyl)phenyl)ethene-1,1,2-triyl)tribenzene

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux

2: sodium azide / dimethyl sulfoxide / 20 °C / Inert atmosphere

With N-Bromosuccinimide; sodium azide; dibenzoyl peroxide; In tetrachloromethane; dimethyl sulfoxide;
DOI:10.1021/ja3064588