1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester

Base Information

Chemical Name:1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester
CAS No.:873056-11-2
Molecular Formula:C₁₆H₂₂N₂O₄
Molecular Weight:306.362
Hs Code.:
Mol file:873056-11-2.mol

Synonyms:1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester

Suppliers and Price of 1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester

Chemical Property:

PSA：75.36000
LogP:4.60580

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester

There total 6 articles about 1(2H)-Quinolinecarboxylic acid, 3,4-dihydro-4,4-diMethyl-7-nitro-, 1,1-diMethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 561297-83-4
4,4-dimethyl-7-nitro-1,2,3,4-tetrahydroquinoline

: 873056-11-2
4,4-dimethyl-7-nitro-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester

Guidance literature:

Reference yield:

: 13209-80-8
N-phenyl-3-methyl-2-butenamide

: 873056-11-2
4,4-dimethyl-7-nitro-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃ / benzene

2: NaOH; LiAlH₄ / tetrahydrofuran; water

3: KNO₃ / sulfuric acid

With NaOH; LiAlH₄; KNO₃; AlCl₃; In tetrahydrofuran; sulfuric acid; water; benzene;

Reference yield:

: 541-47-9
3-Methylbutenoic acid

: 873056-11-2
4,4-dimethyl-7-nitro-3,4-dihydro-2H-quinoline-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride; aniline / dichloromethane; triethylamine

2: AlCl₃ / benzene

3: NaOH; LiAlH₄ / tetrahydrofuran; water

4: KNO₃ / sulfuric acid

With NaOH; thionyl chloride; LiAlH₄; KNO₃; aniline; AlCl₃; In tetrahydrofuran; dichloromethane; sulfuric acid; water; triethylamine; benzene;