(Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE

Base Information

Chemical Name:(Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE
CAS No.:885722-16-7
Molecular Formula:C₃₄H₂₉N₃O₄S
Molecular Weight:575.688
Hs Code.:
Mol file:885722-16-7.mol

Synonyms:(Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE

Suppliers and Price of (Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE

Chemical Property:

PSA：96.74000
LogP:6.61680

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE

There total 6 articles about (Z)-DIMETHYL 1,3-DIBENZYL-2'-(PHENYLIMINO)-1,3-DIHYDRO-2'H-SPIRO[BENZO[D]IMIDAZOLE-2,3'-THIOPHENE]-4',5'-DICARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 762-42-5
dimethyl acetylenedicarboxylate

: 211240-97-0
1,3-dibenzyl-2-N-phenylthiocarbamoylbenzimidazolium inner salt

: 885722-16-7
dimethyl 1,3-dibenzyl-2'-phenylimino-2',3'-dihydrospiro[benzimidazoline-2,3'-thiophene]-4',5'-dicarboxylate

Guidance literature:: In 1,2-dichloro-ethane; at 20 - 30 ℃; for 0.5h;
DOI:10.1039/b517700f

Reference yield: 95.0%

: 1,3-dibenzyl-2-N-phenylthiocarbamoyl benzimidazolium inner salt

: 762-42-5
dimethyl acetylenedicarboxylate

: 885722-16-7
dimethyl 1,3-dibenzyl-2'-phenylimino-2',3'-dihydrospiro(benzimidazoline-2,3'-thiophene)-4',5'-dicarboxylate

: C₃₄H₂₉N₃O₄S

Guidance literature:: In 1,2-dichloro-ethane; at 20 - 30 ℃; for 0.5h;
DOI:10.1002/chem.200601482

Reference yield:

: 1,3-dibenzyl-1H-benzimidazol-3-ium bromide

: 885722-16-7
dimethyl 1,3-dibenzyl-2'-phenylimino-2',3'-dihydrospiro[benzimidazoline-2,3'-thiophene]-4',5'-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaH / tetrahydrofuran; various solvent(s) / 10 - 20 °C

2: 95 percent / 1,2-dichloro-ethane / 0.5 h / 20 - 30 °C

With sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1039/b517700f