dichloro(113C)methanone

Base Information

Chemical Name:dichloro(113C)methanone
CAS No.:53120-07-3
Molecular Formula:CCl₂O
Molecular Weight:99.9054
Hs Code.:
European Community (EC) Number:687-196-7
DSSTox Substance ID:DTXSID30481025
Wikidata:Q82316219
Mol file:53120-07-3.mol

Synonyms:53120-07-3;dichloro(113C)methanone;DTXSID30481025;Phosgene-13C, 99 atom % 13C

Suppliers and Price of dichloro(113C)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Phosgene-13C solution ~1M in benzene, 99 atom %
5ml
$ 497.00

American Custom Chemicals Corporation
PHOSGENE-13C 95.00%
5MG
$ 496.97

Total 1 raw suppliers

Chemical Property of dichloro(113C)methanone

Chemical Property:

Flash Point:4 °C
PSA：17.07000
Density:1.523g/cm³
LogP:1.58400
Storage Temp.:2-8°C
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:98.9359748
Heavy Atom Count:4
Complexity:29

Purity/Quality:

99% ^*data from raw suppliers

Phosgene-13C solution ~1M in benzene, 99 atom % ^*data from reagent suppliers

Safty Information:

Pictogram(s): F,T+
Hazard Codes:F,T+,T
Statements: 11-26-34-48/20-63-65-67-48/23/24/25-36/38-46-45
Safety Statements: 26-28-45-62-53-36/37/39-36/37-16-9

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(=O)(Cl)Cl
Isomeric SMILES:[13C](=O)(Cl)Cl
Uses Phosgene-13C is a labelled form of phosgene, and a useful labelled building block, such as in its use in the synthesis of isotope-labeled metabolites of asenapine.

Technology Process of dichloro(113C)methanone

There total 2 articles about dichloro(113C)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32488-50-9
[⁽¹³⁾C]carbon tetrachloride

: 124-38-9,18923-20-1
carbon dioxide

: 53120-07-3
<¹³C>-phosgene

: 287399-46-6
1,2-(13)C2-tetrachloroethylene

Guidance literature:: With water; at -170.15 ℃; Product distribution; electron beam irradiation;
DOI:10.1039/b204016f

Reference yield:

: 1641-69-6
[13C]Carbon monoxide

: 53120-07-3
<¹³C>-phosgene

Guidance literature:: With Cl₂; In not given; Irradiation (UV/VIS);
DOI:10.1016/0022-2852(89)90162-8

Reference yield:

: 22385-77-9
1-bromo-3,5-di-tert-butylbenzene

: 53120-07-3
<¹³C>-phosgene

: 116186-39-1
<α-¹³C>tris(3,5-di-tert-butylphenyl)methanol

Guidance literature:: With lithium; Yield given. Multistep reaction; 1.) ether, 24 h, 2.) ether/benzene, room temperature, 30 min;
DOI:10.1021/ja00228a010