BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE

Base Information

Chemical Name:BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE
CAS No.:80795-54-6
Molecular Formula:C26H28O5
Molecular Weight:420.505
Hs Code.:
Mol file:80795-54-6.mol

Synonyms:BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE;PHENYLMETHYL 3,5-DI-O-PHENYLMETHYL-BETA-D-RIBOFURANOSIDE

Suppliers and Price of BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE

Chemical Property:

PSA：57.15000
LogP:4.09120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE

There total 5 articles about BENZYL-3,5-DI-O-BENZYL-BETA-D-RIBOFURANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 100-39-0
benzyl bromide

: 55735-86-9
3,5-O-dibenzyloxy-1,2-O-isorpopylidene-α-D-ribofuranose

: 80795-54-6
1,3,5-tri-O-benzyl-α-D-ribofuranose

Guidance literature:: 3,5-O-dibenzyloxy-1,2-O-isorpopylidene-α-D-ribofuranose; With water; trifluoroacetic acid; at 20 ℃;

With di(n-butyl)tin oxide; In methanol; for 1.5h; Heating / reflux;

benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Product distribution / selectivity;

Reference yield:

: 55735-86-9
3,5-O-dibenzyloxy-1,2-O-isorpopylidene-α-D-ribofuranose

: 80795-54-6
1,3,5-tri-O-benzyl-α-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / dioxane / 24 h / 80 °C / Dowex 50W-X₈ (H⁺)

2: 1.) dibutyltin oxide, 2.) potassium carbonate / 1.) methanol, reflux, 1.5 h, 2.) DMF, RT, 12 h

With di(n-butyl)tin oxide; potassium carbonate; In 1,4-dioxane;
DOI:10.1021/jo00347a027

Reference yield:

: 16054-77-6
(3R,4S,5R)-4-(benzyloxy)-5-(benzyloxymethyl)tetrahydrofuran-2,3-diol

: 100-39-0
benzyl bromide

: 80795-54-6
1,3,5-tri-O-benzyl-α-D-ribofuranose

Guidance literature:: (3R,4S,5R)-4-(benzyloxy)-5-(benzyloxymethyl)tetrahydrofuran-2,3-diol; With di(n-butyl)tin oxide; In methanol; for 2h; Heating / reflux;

benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; for 27h; Product distribution / selectivity;