2,5-Dinitro-m-xylene

Base Information

• Chemical Name: 2,5-Dinitro-m-xylene
• CAS No.: 74709-95-8
• Molecular Formula: C8H8N2O4
• Molecular Weight: 0
• Hs Code.: 2904209090
• Mol file: 74709-95-8.mol

Synonyms:2,5-Dinitro-m-xylene;2,6-Dimethyl-1,4-dinitrobenzene

Chemical Property of 2,5-Dinitro-m-xylene

Chemical Property:

• PSA: 91.64000
• LogP: 3.16620

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-Dinitro-m-xylene

There total 8 articles about 2,5-Dinitro-m-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,6-dimethyl-1,4-dinitrosobenzene (157140-38-0) → 2,6-dimethyl-p-dinitrobenzene (74709-95-8)

Guidance literature:

With dihydrogen peroxide; In trifluoroacetic acid; for 10h; Ambient temperature;

Reference yield:

2,6-dimethyl-[1,4]benzoquinone-4-oxime (4965-29-1) → 2,6-dimethyl-p-dinitrobenzene (74709-95-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / hydroxylamine hydrochloride / ethanol / 10 h / Heating

2: 94 percent / NO₂, O₂ / CH₂Cl₂ / 4 h / Ambient temperature

3: 93 percent / 30percent H₂O₂ / trifluoroacetic acid / 10 h / Ambient temperature

With hydroxylamine hydrochloride; dihydrogen peroxide; oxygen; Nitrogen dioxide; In ethanol; dichloromethane; trifluoroacetic acid;

Reference yield:

2,6-dimethyl-1,4-benzoquinone (527-61-7) → 2,6-dimethyl-p-dinitrobenzene (74709-95-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 83 percent / hydroxylamine hydrochloride / ethanol / 24 h / Heating

2: 80 percent / hydroxylamine hydrochloride / ethanol / 10 h / Heating

3: 94 percent / NO₂, O₂ / CH₂Cl₂ / 4 h / Ambient temperature

4: 93 percent / 30percent H₂O₂ / trifluoroacetic acid / 10 h / Ambient temperature

With hydroxylamine hydrochloride; dihydrogen peroxide; oxygen; Nitrogen dioxide; In ethanol; dichloromethane; trifluoroacetic acid;

upstream raw materials:

2,4-dimethyl-3,6-dinitro-aniline

2,6-dimethyl-1,4-dinitrosobenzene

2,6-dimethyl-[1,4]benzoquinone-4-oxime

2,6-dimethyl-1,4-benzoquinone

Downstream raw materials:

1,3-dimethyl-2,4,5-trinitro-benzene

2,6-dimethyl-4-nitroaniline

Refernces