4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE

Base Information

Chemical Name:4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE
CAS No.:69877-88-9
Molecular Formula:C11H15BrO
Molecular Weight:243.1402
Hs Code.:
Mol file:69877-88-9.mol

Synonyms:4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE;2-(BroMoMethyl)-5-Methoxy-1,3,4-triMethyl-benzene

Suppliers and Price of 4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methoxy-2,3,6-trimethylbenzylBromide
250mg
$ 275.00

Medical Isotopes, Inc.
4-Methoxy-2,3,6-trimethylbenzylBromide
100 mg
$ 860.00

American Custom Chemicals Corporation
4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE 95.00%
1G
$ 1593.90

American Custom Chemicals Corporation
4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE 95.00%
100MG
$ 704.55

Total 5 raw suppliers

Chemical Property of 4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE

Chemical Property:

Boiling Point:305.3±37.0 °C(Predicted)
PSA：9.23000
Density:1.267±0.06 g/cm3(Predicted)
LogP:3.51530
Solubility.:Chloroform, Dichloromethane, Tetrahydrofuran

Purity/Quality:

98%Min ^*data from raw suppliers

4-Methoxy-2,3,6-trimethylbenzylBromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4-Methoxy-2,3,6-trimethylbenzyl Bromide (cas# 69877-88-9) is a compound useful in organic synthesis.

Technology Process of 4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE

There total 4 articles about 4-METHOXY-2,3,6-TRIMETHYLBENZYL BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 54344-93-3
(4-methoxy-2,3,6-trimethylphenyl)methanol

: 69877-88-9
2-(bromomethyl)-5-methoxy-1,3,4-trimethylbenzene

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 25 ℃; for 1h;
DOI:10.1002/chem.201403024

Reference yield:

: 54344-92-2
2,3,6-trimethyl-4-methoxy-benzaldehyde

: 69877-88-9
2-(bromomethyl)-5-methoxy-1,3,4-trimethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Na2(OCH₂CH₂OMe)2> / benzene; diethyl ether

2: PBr₃, Py / diethyl ether

With pyridine; phosphorus tribromide; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; benzene;
DOI:10.1021/jm00195a010

Reference yield:

: 20469-61-8
2,3,5-trimethylanisole

: 69877-88-9
2-(bromomethyl)-5-methoxy-1,3,4-trimethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 0.25 h / 10 - 20 °C

1.2: 6 h / 10 - 110 °C

2.1: sodium tetrahydroborate; ethanol / 3 h / 80 °C

3.1: phosphorus tribromide / dichloromethane / 1 h / 0 - 25 °C

With sodium tetrahydroborate; ethanol; phosphorus tribromide; trichlorophosphate; In dichloromethane;
DOI:10.1002/chem.201403024