5-fluoro-2-iodophenol

Base Information

• Chemical Name: 5-fluoro-2-iodophenol
• CAS No.: 186589-87-7
• Molecular Formula: C6H4FIO
• Molecular Weight: 238
• Hs Code.: 2908190090
• Mol file: 186589-87-7.mol

Synonyms:5-fluoro-2-iodophenol;Phenol, 5-fluoro-2-iodo-;2-Hydroxy-4-fluoroiodobenzene;2-Iodo-5-fluorophenol

Chemical Property of 5-fluoro-2-iodophenol

Chemical Property:

• PSA: 20.23000
• LogP: 2.13590

Purity/Quality:

97% ^*data from raw suppliers

5-Fluoro-2-iodophenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-fluoro-2-iodophenol

There total 3 articles about 5-fluoro-2-iodophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-fluoro-1-iodo-2-methoxymethoxy-benzene (1037831-19-8) → 5-fluoro-2-iodo-phenol (186589-87-7)

Guidance literature:

With hydrogenchloride; water; In acetone; at 0 - 20 ℃;

DOI:10.1021/ol800834q

Reference yield:

3-fluorophenol (372-20-3) → 5-fluoro-2-iodo-phenol (186589-87-7)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran

2: BuLi; I₂ / diethyl ether

3: TMSCl; NaI / acetonitrile

With n-butyllithium; chloro-trimethyl-silane; iodine; sodium hydride; sodium iodide; In tetrahydrofuran; diethyl ether; acetonitrile;

DOI:10.1016/S0040-4039(01)01191-1

Reference yield:

1-fluoro-3-(methoxy-methoxy)benzene (126940-10-1) → 5-fluoro-2-iodo-phenol (186589-87-7)

Guidance literature:

Multi-step reaction with 2 steps

1: BuLi; I₂ / diethyl ether

2: TMSCl; NaI / acetonitrile

With n-butyllithium; chloro-trimethyl-silane; iodine; sodium iodide; In diethyl ether; acetonitrile;

DOI:10.1016/S0040-4039(01)01191-1

upstream raw materials:

4-fluoro-1-iodo-2-methoxymethoxy-benzene

3-fluorophenol

1-fluoro-3-(methoxy-methoxy)benzene

Downstream raw materials:

2-(prop-1-ynyl)-benzyl 5-fluoro-2-iodophenyl ether

5-fluoro-2-(prop-1-ynyl)-benzyl 5-fluoro-2-iodophenyl ether

N-[2-(5-fluoro-2-iodophenoxy)phenyl]acetamide

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