(5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester

Base Information

Chemical Name:(5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester
CAS No.:7205-83-6
Molecular Formula:C21H24N2O3
Molecular Weight:218.704
Hs Code.:

Synonyms:(5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester;(5α,6α,7α,12R,19R)-2,3-Didehydro-6,7-epoxyaspidospermidine-3-carboxylic acid methyl ester;Lochnericine;(5alpha,6alpha,7alpha,12R,19alpha)-2,3-Didehydro-6,7-epoxyaspidospermidine-3-carboxylic acid methyl ester

Suppliers and Price of (5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of (5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester

There total 4 articles about (5α,12R,19α)-2,3-Didehydro-6α,7α-epoxyaspidospermidine-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 7205-62-1
1-chloro-4-(isopropylthio)benzene

: 7205-83-6
4-chloro-1-(propane-2-sulphonyl)benzene

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

Reference yield: 77.0%

: 7205-80-3
1-(ethylsulfonyl)-4-chlorobenzene

: 616-38-6
carbonic acid dimethyl ester

: 7205-83-6
4-chloro-1-(propane-2-sulphonyl)benzene

Guidance literature:: With potassium carbonate; at 200 ℃; for 12h;

Reference yield:

: 106-46-7,84348-21-0
para-dichlorobenzene

: 7205-83-6
4-chloro-1-(propane-2-sulphonyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

2: aq. H₂O₂, AcOH

With dihydrogen peroxide; acetic acid;
DOI:10.1021/jo01329a011