2-CHLORO-3',4'-DIMETHYLBENZOPHENONE

Base Information

• Chemical Name: 2-CHLORO-3',4'-DIMETHYLBENZOPHENONE
• CAS No.: 34701-99-0
• Molecular Formula: C15H13ClO
• Molecular Weight: 244.72
• Hs Code.: 2914700090
• Mol file: 34701-99-0.mol

Synonyms:2-CHLORO-3',4'-DIMETHYLBENZOPHENONE;UKRORGSYN-BB BBV-5122424

Chemical Property of 2-CHLORO-3',4'-DIMETHYLBENZOPHENONE

Chemical Property:

• Vapor Pressure: 4.04E-06mmHg at 25°C
• Melting Point: 173 °C
• Boiling Point: 384.6°C at 760 mmHg
• Flash Point: 214.2°C
• PSA: 17.07000
• Density: 1.154g/cm³
• LogP: 4.18780

Purity/Quality:

95% ^*data from raw suppliers

2-Chloro-3',4'-dimethylbenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-3',4'-DIMETHYLBENZOPHENONE

There total 1 articles about 2-CHLORO-3',4'-DIMETHYLBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-Chlor-3',4'-dimethyl-benzophenon (34701-99-0)

Guidance literature:

o-Xylol, 2-Chlor-benzoylchlorid;

DOI:10.1016/S0040-4039(01)97299-5

Reference yield: 45.0%

2-Chlor-3',4'-dimethyl-benzophenon (34701-99-0) + 4-methoxy-aniline (104-94-9) → N-((3,4-dimethyl-phenyl)(2-Chlorophenyl)methylene)-4-methoxyaniline

Guidance literature:

With titanium tetrachloride; triethylamine; In dichloromethane; at 0 - 45 ℃; for 7h; Inert atmosphere;

DOI:10.1002/adsc.201400643

Reference yield:

2-Chlor-3',4'-dimethyl-benzophenon (34701-99-0) + 4-methoxy-aniline (104-94-9) → ((3,4-dimethylphenyl)(2-chlorophenyl)methyl)(4-methoxyphenyl)amine

Guidance literature:

Multi-step reaction with 2 steps

1: titanium tetrachloride; triethylamine / dichloromethane / 7 h / 0 - 45 °C / Inert atmosphere

2: trichlorosilane; N-((1R,2S)-1-hydroxy-1-phenylpropan-2-yl)-N-methylpicolinamide / 1,2-dichloro-ethane / 48 h / 0 °C

With N-((1R,2S)-1-hydroxy-1-phenylpropan-2-yl)-N-methylpicolinamide; trichlorosilane; titanium tetrachloride; triethylamine; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1002/adsc.201400643

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