Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate

Base Information

• Chemical Name: Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate
• CAS No.: 159768-50-0
• Molecular Formula: C9H8FNO5
• Molecular Weight: 229.165
• Hs Code.: 2916310090
• Mol file: 159768-50-0.mol

Synonyms:Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate;4-Fluoro-5-methoxy-2-nitro-benzoic acid methyl ester

Chemical Property of Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate

Chemical Property:

• PSA: 81.35000
• LogP: 2.05230

Purity/Quality:

98%min ^*data from raw suppliers

Methyl 4-fluoro-5-methoxy-2-nitrobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate

There total 4 articles about Methyl 4-fluoro-5-Methoxy-2-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

methyl 4-fluoro-3-methoxy-benzoate (74385-37-8) → methyl 4-fluoro-5-methoxy-2-nitrobenzoate (159768-50-0)

Guidance literature:

With sulfuric acid; nitric acid; for 3h;

DOI:10.1016/j.bmcl.2016.04.028

Reference yield:

sulfuric acid (7664-93-9) + methyl 4-fluoro-3-methoxy-benzoate (74385-37-8) → 2-amino-4-fluoro-5-methoxybenzoic acid methyl ester (159768-51-1) + methyl 4-fluoro-5-methoxy-2-nitrobenzoate (159768-50-0)

Guidance literature:

With nitric acid; palladium; In ethanol;

Reference yield:

4-chloro-7-fluoro-6-methoxyquinazoline (159768-48-6) + sulfuric acid (7664-93-9) + methyl 4-fluoro-3-methoxy-benzoate (74385-37-8) → 2-amino-4-fluoro-5-methoxybenzoic acid methyl ester (159768-51-1) + methyl 4-fluoro-5-methoxy-2-nitrobenzoate (159768-50-0)

Guidance literature:

With nitric acid;

upstream raw materials:

methyl 4-fluoro-3-methoxy-benzoate

4?fluoro-3-methoxybenzoic acid

sulfuric acid

4-chloro-7-fluoro-6-methoxyquinazoline

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