MANDELIC-2,3,4,5,6-D5 ACID

Base Information

Chemical Name:MANDELIC-2,3,4,5,6-D5 ACID
CAS No.:70838-71-0
Molecular Formula:C8H3D5O3
Molecular Weight:157.11
Hs Code.:
Mol file:70838-71-0.mol

Synonyms:MANDELIC-2,3,4,5,6-D5 ACID

Suppliers and Price of MANDELIC-2,3,4,5,6-D5 ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(±)-Mandelic-2,3,4,5,6-d5Acid
100mg
$ 185.00

American Custom Chemicals Corporation
(+/-)-MANDELIC-2,3,4,5,6-D5 ACID 95.00%
5MG
$ 503.55

Total 2 raw suppliers

Chemical Property of MANDELIC-2,3,4,5,6-D5 ACID

Chemical Property:

Melting Point:120-121 °C(Solv: benzene (71-43-2); ethanol (64-17-5))
PSA：57.53000
LogP:0.80460
Storage Temp.:Refrigerator
Solubility.:DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly), Water (Slightly,

Purity/Quality:

97% ^*data from raw suppliers

(±)-Mandelic-2,3,4,5,6-d5Acid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses (±)-Mandelic-2,3,4,5,6-d5 Acid is labelled Mandelic Acid (M162525) which is used as an antiseptic (urinary). Mandelic Acid (M162525) is also used as a short-term exposure biomarker in urine from styrene exposed workers. (±)-Mandelic-2,3,4,5,6-d5 Acid is a labelled Mandelic Acid (M162525) which is used as an antiseptic (urinary). Mandelic Acid (M162525) is also used as a short-term exposure biomarker in urine from styrene exposed workers.

Technology Process of MANDELIC-2,3,4,5,6-D5 ACID

There total 5 articles about MANDELIC-2,3,4,5,6-D5 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 70838-70-9
dichloroacetophenone-d₅

: 70838-71-0
(RS)-2-hydroxy-2-(D₅)phenylacetic acid

Guidance literature:: With water; sodium hydroxide; at 110 ℃; for 0.183333h; Microwave irradiation;
DOI:10.1016/j.tetasy.2014.11.007

Reference yield:

: 70838-72-1
Ethylmandelat-

: 70838-71-0
(RS)-2-hydroxy-2-(D₅)phenylacetic acid

Guidance literature:: With lithium hydroxide; at 20 ℃; for 0.166667h;
DOI:10.1021/acs.orglett.1c02080

Reference yield:

: 1076-43-3
benzene-d6

: 70838-71-0
(RS)-2-hydroxy-2-(D₅)phenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 4 h / 0 °C

2: sodium tetrahydroborate / 1 h / 0 °C

3: lithium hydroxide / 0.17 h / 20 °C

With aluminum (III) chloride; sodium tetrahydroborate; lithium hydroxide; 2: |Friedel-Crafts Acylation;
DOI:10.1021/acs.orglett.1c02080