1-isopropoxy-2-propylbenzene

Base Information

• Chemical Name: 1-isopropoxy-2-propylbenzene
• CAS No.: 20946-00-3
• Molecular Weight: 0
• Mol file: 20946-00-3.mol

Synonyms:1-isopropoxy-2-propylbenzene

Chemical Property of 1-isopropoxy-2-propylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-isopropoxy-2-propylbenzene

There total 1 articles about 1-isopropoxy-2-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodo-propane (75-30-9) + 5-propylphenol (644-35-9) → 2-Isopropoxyphenyl-propane (20946-00-3)

Guidance literature:

Alkaline conditions;

DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

2-Isopropoxyphenyl-propane (20946-00-3) → C26H32N2O3S2 (1374354-69-4)

Guidance literature:

Multi-step reaction with 10 steps

1: aluminum (III) chloride

2: sodium hydride

3: PhMe₂NBr₃

4: sodium diformamide

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

6: Lawessons reagent; pyridine / toluene / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran

8: thionyl chloride / toluene

9: N-ethyl-N,N-diisopropylamine / acetonitrile

10: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; aluminum (III) chloride; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;

DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

2-Isopropoxyphenyl-propane (20946-00-3) → C22H27NO2S2

Guidance literature:

Multi-step reaction with 7 steps

1: aluminum (III) chloride

2: sodium hydride

3: PhMe₂NBr₃

4: sodium diformamide

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

6: Lawessons reagent; pyridine / toluene / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran

With Lawessons reagent; pyridine; aluminum (III) chloride; sodium diformamide; tetrabutyl ammonium fluoride; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; toluene;

DOI:10.1016/j.bmcl.2012.03.067

upstream raw materials:

2-iodo-propane

5-propylphenol

Downstream raw materials:

C₂₆H₃₂N₂O₃S₂

C₂₇H₃₄N₂O₃S₂

C₁₄H₂₀O₂

C₁₄H₂₁NO₂