1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98%

Base Information

• Chemical Name: 1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98%
• CAS No.: 42926-91-0
• Molecular Formula: C13H16O5
• Molecular Weight: 252.267

Synonyms:1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98%;1,6-Anhydro-3-O-(phenylmethyl)-beta-L-idopyranose;1,6-Anhydro-3-O-benzyl-beta-L-idopyranose

Chemical Property of 1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98%

Chemical Property:

• PSA: 68.15000
• LogP: 0.04870

Purity/Quality:

99% ^*data from raw suppliers

1,6-Anhydro-3-O-benzyl-beta-L-idopyranose 98%min ^*data from reagent suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98%

There total 19 articles about 1,6-Anhydro-3-O-benzyl-beta-L-idopyranose min. 98% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

6-O-benzoyl-1,2-O-isopropylidene-3-O-benzyl-5-O-trifluoromethanesulfonyl-α-D-glucofuranose → 3-O-benzyl-1,6-anhydro-β-L-idopyranose (42926-91-0)

Guidance literature:

With sodium methylate; In methanol; chloroform; at 20 - 90 ℃; for 30h;

Reference yield: 72.0%

benzaldehyde (100-52-7) + 1,6-anhydro-2,3,4-triO-trimethylsilyl-β-L-idopyranose (334834-37-6) → 3-O-benzyl-1,6-anhydro-β-L-idopyranose (42926-91-0)

Guidance literature:

With triethylsilane; trimethylsilyl trifluoromethanesulfonate;

DOI:10.1002/jccs.200400175

Reference yield: 71.0%

5,6-anhydro-3-O-benzyl-1,2-O-isopropylidene-β-L-idofuranose (37776-17-3) → 3-O-benzyl-1,6-anhydro-β-L-idopyranose (42926-91-0)

Guidance literature:

With sulfuric acid; water; In 1,4-dioxane; for 22h; Reflux;

DOI:10.1039/c1ob06415k

upstream raw materials:

benzaldehyde

1,6-anhydro-2,3,4-triO-trimethylsilyl-β-L-idopyranose

6-O-benzoyl-3-O-benzyl-1,2-O-isopropylidene-5-O-methanesulfonyl-α-D-glucofuranose

Benzoic acid (S)-2-((3aR,5S,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-methanesulfonyloxy-ethyl ester

Downstream raw materials:

1,6-anhydro-2-O-benzoyl-3-O-benzyl-β-L-idopyranoside

Trifluoro-methanesulfonic acid (1S,2R,3S,4R,5S)-3-benzyloxy-2-trifluoromethanesulfonyloxy-6,8-dioxa-bicyclo[3.2.1]oct-4-yl ester

methyl 4-O-(2-azido-4-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-O-benzyl-α-L-idopyranosiduronic acid

methyl 4-O-(2-azido-4-O-benzyl-2-deoxy-3,6-di-O-sulfonato-α-D-glucopyranosyl)-3-O-benzyl-2-O-sulfonato-α-L-idopyranosiduronic acid

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