3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide

Base Information

• Chemical Name: 3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide
• CAS No.: 21411-21-2
• Molecular Formula: C19H22INO4
• Molecular Weight: 455.292
• Mol file: 21411-21-2.mol

Synonyms:1,2-Dehydro Reticuline Iodide;1,2-Dehydroreticuline Iodide;3,4-Dihydro-7-hydroxy-1-(3-hydroxy-4-Methoxybenzyl)-6-Methoxy-2-MethylisoquinoliniuM Iodide;3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide

Chemical Property of 3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide

Chemical Property:

• Melting Point: 198-200 °C
• PSA: 64.76000
• LogP: 3.74040
• Storage Temp.: -20°C Freezer
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

1,2-DehydroReticulineIodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 1,2-Dehydro Reticuline Iodide is a dehydro iminium salt derivative of Reticuline (R188500) and a precursor in the synthesis of Multifloramine.

Technology Process of 3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide

There total 3 articles about 3,4-Dihydro-7-hydroxy-1-[(3-hydroxy-4-Methoxyphenyl)Methyl]-6-Methoxy-2-MethylisoquinoliniuM Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-Norreticuline (4781-58-2) → 1,2-dehydroreticulinium iodide (21411-21-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 10 mg / borate, ascorbate, (NH₄)2SO₄ (pH 8.9) / H₂O / 30 °C / enzym fraction from Berberis stolonifera cell cultures

2: 7 mg / dimethylsulfoxide / 24 h / Ambient temperature

With ammonium sulfate; boric acid; ascorbic acid; In water; dimethyl sulfoxide;

DOI:10.1016/0031-9422(92)80020-F

Reference yield:

1,2-dehydronorreticuline (72258-91-4) + methyl iodide (74-88-4) → 1,2-dehydroreticulinium iodide (21411-21-2)

Guidance literature:

In dimethyl sulfoxide; for 24h; Ambient temperature;

DOI:10.1016/0031-9422(92)80020-F

Reference yield:

→ 1,2-dehydroreticulinium iodide (21411-21-2)

Guidance literature:

7-Hydroxy-6-methoxy-1-(3-hydroxy-4-methoxy-benzyl)-3,4-dihydro-isochinolin-hydrochlorid, Methyljodid/OH^-;

upstream raw materials:

1,2-dehydronorreticuline

methyl iodide

(-)-Norreticuline

Downstream raw materials:

(R)-reticuline

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