4-allyl-4-Methylcyclohexanone

Base Information

Chemical Name:4-allyl-4-Methylcyclohexanone
CAS No.:117360-99-3
Molecular Formula:C₁₀H₁₆O
Molecular Weight:152.236
Hs Code.:
Mol file:117360-99-3.mol

Synonyms:4-allyl-4-Methylcyclohexanone

Suppliers and Price of 4-allyl-4-Methylcyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Methyl-4-(2-propen-1-yl)-cyclohexanone
50mg
$ 240.00

TRC
4-Methyl-4-(2-propen-1-yl)-cyclohexanone
10mg
$ 65.00

Total 3 raw suppliers

Chemical Property of 4-allyl-4-Methylcyclohexanone

Chemical Property:

PSA：17.07000
LogP:2.71190

Purity/Quality:

98%min ^*data from raw suppliers

4-Methyl-4-(2-propen-1-yl)-cyclohexanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-allyl-4-Methylcyclohexanone

There total 4 articles about 4-allyl-4-Methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 13481-16-8
4-methyl-4-(prop-2-enyl)cyclohex-2-en-1-one

: 117360-99-3
4-methyl-4-(2-propenyl)cyclohexanone

Guidance literature:: With lithium; tert-butyl alcohol; In tetrahydrofuran; ammonia; for 0.5h; Heating;
DOI:10.1002/hlca.19880710120

Reference yield:

: 117360-96-0
3-<(1-methylpropyl)oxy>-2-cyclohexen-1-one

: 117360-99-3
4-methyl-4-(2-propenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) (i-Pr)2NH, BuLi / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, -78 deg C to room temperature

2: 1.) LDA, 2.) HMPA / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, room temperature, 30 min

3: 1.) LiAlH₄, 2.) 25percent H₂SO₄ / 1.) ether, 0 deg C, 2.) ether, water, 0 deg C, 30 min

4: 85 percent / t-BuOH, Li / tetrahydrofuran; liquid ammonia / 0.5 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; lithium; diisopropylamine; tert-butyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; ammonia;
DOI:10.1002/hlca.19880710120

Reference yield:

: 117360-97-1
3-<(1-methylpropyl)oxy>-6-(2-propenyl)-2-cyclohexen-1-one

: 117360-99-3
4-methyl-4-(2-propenyl)cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA, 2.) HMPA / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, room temperature, 30 min

2: 1.) LiAlH₄, 2.) 25percent H₂SO₄ / 1.) ether, 0 deg C, 2.) ether, water, 0 deg C, 30 min

3: 85 percent / t-BuOH, Li / tetrahydrofuran; liquid ammonia / 0.5 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sulfuric acid; lithium; tert-butyl alcohol; lithium diisopropyl amide; In tetrahydrofuran; ammonia;
DOI:10.1002/hlca.19880710120