.beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate

Base Information

• Chemical Name: .beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate
• CAS No.: 165874-19-1
• Molecular Formula: C19H25NO8S
• Molecular Weight: 427.47
• Mol file: 165874-19-1.mol

Synonyms:.beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate

Chemical Property of .beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate

Chemical Property:

• Melting Point: 202 - 203 °C (methanol)
• Boiling Point: 668.8±55.0 °C(Predicted)
• PKA: 13.60±0.70(Predicted)
• PSA: 117.77000
• Density: 1.34±0.1 g/cm3(Predicted)
• LogP: 2.34930

Purity/Quality:

Safty Information:

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Technology Process of .beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate

There total 1 articles about .beta.-D-Glucopyranoside, 2-propenyl 2-(acetylamino)-2-deoxy-4,6-O-(phenylmethylene)-, 3-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

allyl 2-deoxy-2-acetamido-4,6-O-benzylidene-β-D-glucopyranoside (65947-37-7) + methanesulfonyl chloride (124-63-0) → allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-β-D-glucopyranoside (165874-19-1)

Guidance literature:

In pyridine; at 4 ℃; for 16h;

Reference yield: 91.0%

allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-β-D-glucopyranoside (165874-19-1) → allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside (165874-21-5)

Guidance literature:

With sodium acetate; In 2-methoxy-ethanol; water; at 125 ℃; for 9h;

Reference yield: 73.0%

allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-β-D-glucopyranoside (165874-19-1) → allyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-β-D-allopyranoside

Guidance literature:

With sodium isopropylate; In 1,4-dioxane; isopropyl alcohol; for 0.5h; Heating;

DOI:10.1016/S0957-4166(00)80385-7

upstream raw materials:

allyl 2-deoxy-2-acetamido-4,6-O-benzylidene-β-D-glucopyranoside

methanesulfonyl chloride

Downstream raw materials:

allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside

allyl 2,3-dideoxy-2,3-(N-p-toluenesulfonylepimino)-β-D-allopyranoside

allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside

3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-allopyranose

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