2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI)

Base Information

• Chemical Name: 2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI)
• CAS No.: 224967-43-5
• Molecular Formula: C₁₁H₁₈O
• Molecular Weight: 166.263
• Mol file: 224967-43-5.mol

Synonyms:2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI)

Chemical Property of 2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI)

Chemical Property:

• PSA: 17.07000
• LogP: 2.95790

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI)

There total 6 articles about 2-Cyclohexen-1-one,2,3-dimethyl-5-(1-methylethyl)-,(5R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

Carvone (99-49-0,22327-39-5) + methylmagnesium bromide (75-16-1) → 5-isopropyl-2,3-dimethylcyclohex-2-enone (224967-43-5)

Guidance literature:

Carvone; methylmagnesium bromide; In diethyl ether; at 0 - 20 ℃; for 2h;

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ol503176y

Reference yield: 19.0%

(R)-5-Isopropyl-1,2-dimethyl-cyclohex-2-enol (1072085-41-6) → (S)-6-methylcarvone (85710-66-3,224967-43-5)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodosylbenzene; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

DOI:10.1055/s-2008-1078500

Reference yield:

(1RS,5S)-1-hydroxy-1,2-dimethyl-5-(2-propyl)-2-cyclohexene (224967-39-9) → (S)-2,3-dimethyl-5-(2-propyl)-2-cyclohexenone (224967-43-5)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 12h; Yield given; Ambient temperature;

DOI:10.1021/ja9843122

upstream raw materials:

Carvone

methylmagnesium bromide

(R)-5-Isopropyl-1,2-dimethyl-cyclohex-2-enol

(1RS,5S)-1-hydroxy-1,2-dimethyl-5-(2-propyl)-2-cyclohexene

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