2,4-Dinitrophenyl 2-tert-butylphenyl ether

Base Information

• Chemical Name: 2,4-Dinitrophenyl 2-tert-butylphenyl ether
• CAS No.: 32101-58-9
• Molecular Formula: C16H16N2O5
• Molecular Weight: 316.31
• Hs Code.: 2909309090
• Mol file: 32101-58-9.mol

Synonyms:1-[2-(1,1-Dimethylethyl)phenoxy]-2,4-dinitrobenzene;2,4-Dinitrophenyl 2-tert-butylphenyl ether;o-tert-Butylphenyl 2,4-dinitrophenyl ether

Chemical Property of 2,4-Dinitrophenyl 2-tert-butylphenyl ether

Chemical Property:

• PSA: 100.87000
• LogP: 5.63920

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-Dinitrophenyl 2-tert-butylphenyl ether

There total 2 articles about 2,4-Dinitrophenyl 2-tert-butylphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-tert-butylphenyl tert-butyldimethylsilyl ether + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 2-tert-butyl-2',4'-dinitro-diphenylether (32101-58-9)

Guidance literature:

With P(i-BuNCH₂CH₂)3N; In toluene; at 180 ℃; for 3h; microwave irradiation;

DOI:10.1016/j.tetlet.2008.03.089

Reference yield:

→ 2-tert-butyl-2',4'-dinitro-diphenylether (32101-58-9)

Guidance literature:

entspr. Phenol, 2,4-Dinitrofluorbenzol;

DOI:10.1016/S0003-2670(01)82133-4

upstream raw materials:

2,4-Dinitrofluorobenzene

Refernces