[2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER

Base Information

Chemical Name:[2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER
CAS No.:913642-59-8
Molecular Formula:C14H21NO4
Molecular Weight:267.323
Hs Code.:
Mol file:913642-59-8.mol

Synonyms:[2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER;N-Boc-2-hydroxy-2-(3-Methoxyphenyl)ethanaMine;tert-butyl 2-hydroxy-2-(3-methoxyphenyl)ethylcarbamate;CARBAMIC ACID, [2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-, 1,1-DIMETHYLETHYL ESTER (9Cl)

Suppliers and Price of [2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
CARBAMICACID,[2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-,1,1-DIMETHYLETHYLESTER(9Cl) 95
25g
$ 3025.00

Acrotein
N-Boc-2-hydroxy-2-(3-methoxyphenyl)ethanamine 97%
0.5g
$ 174.17

Total 2 raw suppliers

Chemical Property of [2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER

Chemical Property:

PSA：67.79000
LogP:2.64420

Purity/Quality:

95%-98% ^*data from raw suppliers

CARBAMICACID,[2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-,1,1-DIMETHYLETHYLESTER(9Cl) 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER

There total 3 articles about [2-HYDROXY-2-(3-METHOXYPHENYL)ETHYL]-CARBAMIC ACID 1,1-DIMETHYLETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 27382-18-9
2-amino-1-(3-methoxyphenyl)ethanol

: 913642-59-8
tert-butyl (2-hydroxy-2-(3-methoxyphenyl)ethyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 25 ℃; for 2.16667h;
DOI:10.1002/anie.201507630

Reference yield:

: 626-20-0
3-methoxystyrene

: 913642-59-8
tert-butyl (2-hydroxy-2-(3-methoxyphenyl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: O-pivaloylhydroxylamine trifluoromethanesulfonate salt; (phthalocyaninato)iron(II) / acetonitrile; water / 16 h / 25 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2.17 h / 0 - 25 °C

With (phthalocyaninato)iron(II); O-pivaloylhydroxylamine trifluoromethanesulfonate salt; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1002/anie.201507630