4'-Nitrobiphenyl-4-sulfonyl chloride

Base Information

Chemical Name:4'-Nitrobiphenyl-4-sulfonyl chloride
CAS No.:20443-75-8
Molecular Formula:C12H8ClNO4S
Molecular Weight:297.719
Hs Code.:2904909090
European Community (EC) Number:673-509-4
DSSTox Substance ID:DTXSID30375056
Wikidata:Q82163599
Mol file:20443-75-8.mol

Synonyms:4'-nitrobiphenyl-4-sulfonyl chloride;20443-75-8;4'-Nitro-biphenyl-4-sulfonyl chloride;4-(4-nitrophenyl)benzenesulfonyl Chloride;4'-Nitro-[1,1'-biphenyl]-4-sulfonyl chloride;SCHEMBL848452;DTXSID30375056;ITVYADZNMWHYOW-UHFFFAOYSA-N;4'-nitro-1,1'-biphenyl-4-sulfonyl chloride;4'-nitrobiphenyl-4-sulfonyl chloride, AldrichCPR;J-013325;HEXAHYDRO-2-[(4-METHOXYLPHENYL)METHYL]-1H-AZEPINE

Suppliers and Price of 4'-Nitrobiphenyl-4-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Oakwood
4'-Nitro-biphenyl-4-sulfonylchloride
1g
$ 444.00

Crysdot
4'-Nitro-[1,1'-biphenyl]-4-sulfonylchloride 95+%
1g
$ 418.00

CHESS?
SB000106:4'-Nitro-biphenyl-4-sulfonylchloride 95
5 g
$ 1020.00

American Custom Chemicals Corporation
4'-NITROBIPHENYL-4-SULFONYL CHLORIDE 95.00%
1G
$ 1280.66

AHH
4-Nitrobiphenyl-4-sulfonylchloride 98%
1g
$ 260.00

Total 8 raw suppliers

Chemical Property of 4'-Nitrobiphenyl-4-sulfonyl chloride

Chemical Property:

Boiling Point:447.8±28.0 °C(Predicted)
PSA：88.34000
Density:1.464±0.06 g/cm3(Predicted)
LogP:4.79330
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:296.9862566
Heavy Atom Count:19
Complexity:412

Purity/Quality:

98%min ^*data from raw suppliers

4'-Nitro-biphenyl-4-sulfonylchloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:C,N
Statements: 20/21/22-34-37-51/53
Safety Statements: 26-36/37/39-45-61

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C2=CC=C(C=C2)S(=O)(=O)Cl)[N+](=O)[O-]

Technology Process of 4'-Nitrobiphenyl-4-sulfonyl chloride

There total 6 articles about 4'-Nitrobiphenyl-4-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 91493-72-0
4-nitrobiphenylsulfonic acid

: 20443-75-8
4'-nitrobiphenyl-4-sulfonyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; for 4h; Heating / reflux;

Reference yield:

: 92-93-3
1-phenyl-4-nitrobenzene

: 20443-75-8
4'-nitrobiphenyl-4-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ClSO₃H / CHCl₃ / 20 °C

2: SOCl₂ / dimethylformamide / Heating

With chlorosulfonic acid; thionyl chloride; In chloroform; N,N-dimethyl-formamide; 1: sulfonation / 2: Chlorination;
DOI:10.1021/jm9903141

Reference yield:

: 92-93-3
1-phenyl-4-nitrobenzene

: 20443-75-8
4'-nitrobiphenyl-4-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ClSO₃H / CHCl₃ / 60 °C

2: SOCl₂ / Heating

With chlorosulfonic acid; thionyl chloride; In chloroform;
DOI:10.1016/j.bmcl.2005.06.019