2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)

Base Information

Chemical Name:2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)
CAS No.:277751-22-1
Molecular Formula:C₈H₁₀O₃
Molecular Weight:154.166
Hs Code.:
Mol file:277751-22-1.mol

Synonyms:2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)

Suppliers and Price of 2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)

Chemical Property:

Boiling Point:233.5±40.0 °C(Predicted)
PSA：43.37000
Density:1.241±0.06 g/cm3(Predicted)
LogP:0.69470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI)

There total 4 articles about 2-Cyclopentene-1-carboxylic acid, 2-formyl-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 30758-76-0
(+/-)-2-formylcyclopent-2-enecarboxylic acid

: 149-73-5
trimethyl orthoformate

: 277751-22-1
(+/-)-2-formylcyclopent-2-enecarboxylic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1021/jm990557t

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 277751-22-1
(+/-)-2-formylcyclopent-2-enecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / hexane / 20 °C

1.2: 22 percent / aq. NaHCO₃ / 4 h / 75 °C

2.1: 72 percent / p-TsOH / 72 h

With toluene-4-sulfonic acid; triethylamine; In hexane;
DOI:10.1021/jm049503w

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 277751-22-1
(+/-)-2-formylcyclopent-2-enecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / hexane

2: aq. NaHCO₃ / 5 h / 75 °C

3: 97 percent / p-toluenesulfonic acid monohydrate

With sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; In hexane; 1: Addition / 2: Hydrolysis / 3: Esterification;
DOI:10.1021/jm990557t