2-Bromoisonicotinohydrazide

Base Information

• Chemical Name: 2-Bromoisonicotinohydrazide
• CAS No.: 29849-15-8
• Molecular Formula: C6H6BrN3O
• Molecular Weight: 216.037
• Hs Code.: 2933399090
• Mol file: 29849-15-8.mol

Synonyms:2-Bromoisonicotinohydrazide;2-Bromoisonicotinohydrazide 98%;2-Bromopyridine-4-carbohydrazide, 2-Bromoisonicotinic acid hydrazide

Chemical Property of 2-Bromoisonicotinohydrazide

Chemical Property:

• PSA: 68.01000
• LogP: 1.53880
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Bromoisonicotinohydrazide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Bromoisonicotinohydrazide

There total 3 articles about 2-Bromoisonicotinohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoisonicotinic acid (66572-56-3) → 2-bromoisonicotinic acid hydrazide (29849-15-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: ethanol; N₂H₄+H₂O

With diethyl ether; ethanol; hydrazine hydrate;

DOI:10.1021/ja01104a046

Reference yield:

methyl 2-bromoisonicotinate (26156-48-9) → 2-bromoisonicotinic acid hydrazide (29849-15-8)

Guidance literature:

With ethanol; hydrazine hydrate;

DOI:10.1021/ja01104a046

Reference yield:

→ 2-bromoisonicotinic acid hydrazide (29849-15-8)

Guidance literature:

2-Brom-isonicotinsaeure-ethylester (in A.), 70percentig. N2H4*H2O (Siedetemp., 2h);

upstream raw materials:

methyl 2-bromoisonicotinate

2-bromoisonicotinic acid