ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE

Base Information

• Chemical Name: ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE
• CAS No.: 107774-17-4
• Molecular Formula: C₁₃H₁₅ClO₄
• Molecular Weight: 270.713
• Hs Code.: 2918990090
• Mol file: 107774-17-4.mol

Synonyms:ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE

Chemical Property of ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE

Chemical Property:

• Vapor Pressure: 1.93E-06mmHg at 25°C
• Boiling Point: 394.8°C at 760 mmHg
• Flash Point: 158.1°C
• PSA: 52.60000
• Density: 1.195g/cm³
• LogP: 2.87460

Purity/Quality:

97% ^*data from raw suppliers

Ethyl4-(5-Chloro-2-methoxyphenyl)-4-oxobutanoate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE

There total 5 articles about ETHYL 4-(5-CHLORO-2-METHOXYPHENYL)-4-OXOBUTANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloromethoxybenzene (623-12-1) → 4-(5-chloro-2-methoxy-phenyl)-4-oxo-butyric acid ethyl ester (107774-17-4)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃

2: HBr; acetic acid

4: Methylierung

With aluminium trichloride; hydrogen bromide; acetic acid;

Reference yield:

5-chloro-2-methoxy-γ-oxobenzenebutanoic acid (63213-94-5) → 4-(5-chloro-2-methoxy-phenyl)-4-oxo-butyric acid ethyl ester (107774-17-4)

Guidance literature:

Multi-step reaction with 3 steps

1: HBr; acetic acid

3: Methylierung

With hydrogen bromide; acetic acid;

Reference yield:

4-chloro-phenol (106-48-9,82344-39-6) → 4-(5-chloro-2-methoxy-phenyl)-4-oxo-butyric acid ethyl ester (107774-17-4)

Guidance literature:

Multi-step reaction with 3 steps

1: AlCl₃

3: Methylierung

With aluminium trichloride;

upstream raw materials:

4-(5-chloro-2-hydroxy-phenyl)-4-oxo-butyric acid ethyl ester

4-chloromethoxybenzene

4-(5-Chloro-2-hydroxyphenyl)-4-oxobutanoic Acid

5-chloro-2-methoxy-γ-oxobenzenebutanoic acid

Downstream raw materials:

5-(5-chloro-2-methoxy-phenyl)-dihydro-furan-2-one

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