3-(4-AMINO-PHENYL)-PYRROLIDINE-2,5-DIONE

Base Information

• Chemical Name: 3-(4-AMINO-PHENYL)-PYRROLIDINE-2,5-DIONE
• CAS No.: 32856-49-8
• Molecular Formula: C10H10 N2 O2
• Molecular Weight: 190.202
• Hs Code.: 2925190090
• Mol file: 32856-49-8.mol

Synonyms:Succinimide,2-(p-aminophenyl)- (8CI); (?à)-3-(4-Aminophenyl)-2,5-pyrrolidinedione; WSP 3

Chemical Property of 3-(4-AMINO-PHENYL)-PYRROLIDINE-2,5-DIONE

Chemical Property:

• Vapor Pressure: 7.47E-09mmHg at 25°C
• Boiling Point: 465.8°C at 760 mmHg
• Flash Point: 235.5°C
• PSA: 72.19000
• Density: 1.318g/cm³
• LogP: 1.30890

Purity/Quality:

97% ^*data from raw suppliers

3-(4-Amino-phenyl)-pyrrolidine-2,5-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 36/37/38-43-22
• Safety Statements: 26-36/37/39-36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(4-AMINO-PHENYL)-PYRROLIDINE-2,5-DIONE

There total 4 articles about 3-(4-AMINO-PHENYL)-PYRROLIDINE-2,5-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-(4-nitrophenyl)-pyrrolidine-2,5-dione (32856-95-4) → 3-(4-amino-phenyl)-pyrrolidine-2,5-dione (32856-49-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/jm00154a016

Reference yield:

3-phenylpyrrolidine-2,5-dione (3464-18-4) → 3-(4-amino-phenyl)-pyrrolidine-2,5-dione (32856-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / HNO₃ / -40 °C

2: 90 percent / H₂ / 10percent Pd/C / ethyl acetate

With hydrogen; nitric acid; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/jm00154a016

Reference yield:

2-phenylsuccinic acid (635-51-8,10424-29-0) → 3-(4-amino-phenyl)-pyrrolidine-2,5-dione (32856-49-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 60 percent / urea / 0.5 h / 180 - 200 °C

2: 63 percent / HNO₃ / -40 °C

3: 90 percent / H₂ / 10percent Pd/C / ethyl acetate

With hydrogen; nitric acid; urea; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/jm00154a016

upstream raw materials:

3-(4-nitrophenyl)-pyrrolidine-2,5-dione

3-phenylpyrrolidine-2,5-dione

2-phenylsuccinic acid

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