CYCLOHEPTANESULFONYL CHLORIDE

Base Information

• Chemical Name: CYCLOHEPTANESULFONYL CHLORIDE
• CAS No.: 187143-10-8
• Molecular Formula: C₇H₁₃ClO₂S
• Molecular Weight: 196.698
• Hs Code.: 2904909090
• Mol file: 187143-10-8.mol

Synonyms:CYCLOHEPTANESULFONYL CHLORIDE

Chemical Property of CYCLOHEPTANESULFONYL CHLORIDE

Chemical Property:

• PSA: 42.52000
• LogP: 3.35860
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

CycloheptanesulfonylChloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOHEPTANESULFONYL CHLORIDE

There total 2 articles about CYCLOHEPTANESULFONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

cycloheptyl thioacetate → cycloheptylsulfonyl chloride (187143-10-8)

Guidance literature:

With hydrogenchloride; N-chloro-succinimide; In water; acetonitrile; at 0 - 15 ℃; for 2.5h; Reagent/catalyst; Solvent; Temperature;

Reference yield:

cycloheptanol (502-41-0) → cycloheptylsulfonyl chloride (187143-10-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 0 - 10 °C

2: tetrahydrofuran / 4 h / 20 - 30 °C

3: N-chloro-succinimide; hydrogenchloride / water; acetonitrile / 2.5 h / 0 - 15 °C

With hydrogenchloride; N-chloro-succinimide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;

upstream raw materials:

cycloheptanol

Refernces