(+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene

Base Information

Chemical Name:(+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene
CAS No.:60598-98-3
Molecular Formula:C₃₆H₃₄O₃
Molecular Weight:514.664
Hs Code.:
Mol file:60598-98-3.mol

Synonyms:(+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene;[R,(+)]-1-O,2-O-Dibenzyl-3-O-trityl-L-glycerol

Suppliers and Price of (+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene

Chemical Property:

Melting Point:81 - 82 °C (ethanol)
PSA：27.69000
LogP:7.79730

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene

There total 4 articles about (+)-1,1',1''-[[(R)-2,3-Di(benzyloxy)propoxy]methylidyne]trisbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 20196-71-8
(2S)-2,3-bis(benzyloxy)propanol

: 76-83-5
trityl chloride

: 60598-98-3
1,2-di-O-benzyl-3-O-triphenylmethyl-sn-glycerol

Guidance literature:: With pyridine; for 96h; Ambient temperature;
DOI:10.1021/jm00145a014

Reference yield:

: 20196-69-4
1,2,5,6-tetra-O-benzyl-D-mannitol

: 60598-98-3
1,2-di-O-benzyl-3-O-triphenylmethyl-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaIO₄, NaOMe / methanol / 24 h / Ambient temperature

2: 71 percent / NaBH₄ / methanol

3: 71 percent / pyridine / 96 h / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium periodate; sodium methylate; In methanol;
DOI:10.1021/jm00145a014

Reference yield:

: 20196-70-7
(+)-(R)-2,3-bis(benzyloxy)propanal

: 60598-98-3
1,2-di-O-benzyl-3-O-triphenylmethyl-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NaBH₄ / methanol

2: 71 percent / pyridine / 96 h / Ambient temperature

With pyridine; sodium tetrahydroborate; In methanol;
DOI:10.1021/jm00145a014