2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide

Base Information

Chemical Name:2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide
CAS No.:76120-22-4
Molecular Formula:C₁₇H₁₆Cl₂N₂O₅
Molecular Weight:399.23
Hs Code.:
DSSTox Substance ID:DTXSID80601973
Nikkaji Number:J9.842F
Mol file:76120-22-4.mol

Synonyms:76120-22-4;2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide;SCHEMBL133575;DTXSID80601973;2-[5-(2,4-Dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropionamide

Suppliers and Price of 2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide

Chemical Property:

Boiling Point:564.0±50.0 °C(Predicted)
PKA:14.82±0.46(Predicted)
PSA：96.87000
Density:1.366±0.06 g/cm3(Predicted)
LogP:5.96080
XLogP3:4.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:398.0436270
Heavy Atom Count:26
Complexity:490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCNC(=O)C(C)OC1=C(C=CC(=C1)OC2=C(C=C(C=C2)Cl)Cl)[N+](=O)[O-]
Uses Etnipromid is used in herbicidal compositions.

Technology Process of 2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide

There total 10 articles about 2-[5-(2,4-dichlorophenoxy)-2-nitrophenoxy]-N-ethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.7%

: 75-04-7,85404-22-4
ethylamine

: 62122-44-5
2-<5-(2',4'-Dichlorphenoxy)-2-nitrophenoxy>-propionsaeureethylester

: 76120-22-4
2-<5-(2',4'-Dichlorphenoxy)-2-nitrophenoxy>-propionsaeureethylamid

Guidance literature:: In water; at 50 ℃; for 1h;
DOI:10.1515/znb-1980-0721

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 76120-22-4
2-<5-(2',4'-Dichlorphenoxy)-2-nitrophenoxy>-propionsaeureethylamid

Guidance literature:: Multi-step reaction with 4 steps

1: 96.5 percent / K₂CO₃ / dimethylsulfoxide / 8.5 h / 140 °C

2: 94.3 percent / 40percent NaOH / 4 h / Heating

3: 88 percent / K₂CO₃ / butan-2-one / 15 h / Heating

4: 82.7 percent / H₂O / 1 h / 50 °C

With sodium hydroxide; potassium carbonate; In water; dimethyl sulfoxide; butanone;
DOI:10.1515/znb-1980-0721

Reference yield:

: 6627-53-8
1-chloro-3-methoxy-4-nitrobenzene

: 76120-22-4
2-<5-(2',4'-Dichlorphenoxy)-2-nitrophenoxy>-propionsaeureethylamid

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / K₂CO₃ / dimethylsulfoxide / 5 h / 150 °C

2: 51 percent / 48percent HBr / acetic acid / 12 h / Heating

3: 88 percent / K₂CO₃ / butan-2-one / 15 h / Heating

4: 82.7 percent / H₂O / 1 h / 50 °C

With hydrogen bromide; potassium carbonate; In water; acetic acid; dimethyl sulfoxide; butanone;
DOI:10.1515/znb-1980-0721