1-Bromo-4-iodo-2,5-dimethylbenzene

Base Information

Chemical Name:1-Bromo-4-iodo-2,5-dimethylbenzene
CAS No.:699119-05-6
Molecular Formula:C8H8BrI
Molecular Weight:310.96
Hs Code.:2903999090
DSSTox Substance ID:DTXSID10598680
Nikkaji Number:J3.204.658D
Wikidata:Q82494464
Mol file:699119-05-6.mol

Synonyms:699119-05-6;1-BROMO-4-IODO-2,5-DIMETHYLBENZENE;1-bromo-2,5-dimethyl-4-iodobenzene;2-Bromo-5-iodo-p-xylene;Benzene, 1-bromo-4-iodo-2,5-dimethyl-;SCHEMBL8983421;4-Bromo-2,5-Dimethyliodobenzene;DTXSID10598680;AMY28455;MFCD07780644;AKOS025395465;1-Bromo-4-iodo-2,5-dimethyl-benzene;AS-83220;DB-103161;CS-0144667;C13539;A855522

Suppliers and Price of 1-Bromo-4-iodo-2,5-dimethylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Oakwood
2-Bromo-5-iodo-p-xylene 97%
1g
$ 70.00

Crysdot
1-Bromo-4-iodo-2,5-dimethylbenzene 95+%
10g
$ 332.00

AOBChem
1-Bromo-2,5-dimethyl-4-iodobenzene 97%
1g
$ 61.00

American Custom Chemicals Corporation
2-BROMO-5-IODO-PARA-XYLENE 95.00%
5MG
$ 495.73

Alichem
1-Bromo-2,5-dimethyl-4-iodobenzene
1g
$ 1549.60

Alichem
1-Bromo-2,5-dimethyl-4-iodobenzene
500mg
$ 839.45

Alichem
1-Bromo-2,5-dimethyl-4-iodobenzene
250mg
$ 470.40

Total 10 raw suppliers

Chemical Property of 1-Bromo-4-iodo-2,5-dimethylbenzene

Chemical Property:

PSA：0.00000
LogP:3.67050
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:309.88541
Heavy Atom Count:10
Complexity:116

Purity/Quality:

97% ^*data from raw suppliers

2-Bromo-5-iodo-p-xylene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1I)C)Br

Technology Process of 1-Bromo-4-iodo-2,5-dimethylbenzene

There total 8 articles about 1-Bromo-4-iodo-2,5-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1074-24-4
2,5-dibromo-p-xylene

: 699119-05-6
1-bromo-4-iodo-2,5-dimethylbenzene

Guidance literature:: 2,5-dibromo-p-xylene; With n-butyllithium; In tetrahydrofuran; hexane;

With 1,2-Diiodoethane; In tetrahydrofuran; hexane; at -60 - 20 ℃;
DOI:10.1002/anie.200501368

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 699119-05-6
1-bromo-4-iodo-2,5-dimethylbenzene

: 1318254-95-3
9-(4-bromophenyl)-2,6-dichloro-9H-purine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / 30 h / 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; caesium carbonate / ethanol; toluene / 24 h / 73 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; caesium carbonate; diisopropylamine; In ethanol; toluene; 1: Sonogashira coupling / 2: Suzuki coupling;
DOI:10.1021/ic201092s

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 1228259-49-1
9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluoro-6-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)tetradec-1-yne

: 699119-05-6
1-bromo-4-iodo-2,5-dimethylbenzene

: 1318254-95-3
9-(4-bromophenyl)-2,6-dichloro-9H-purine

: 1228259-50-4
1-bromo-4-[9,9,10,10,11,11,12,12,13,13,14,14,14-tridecafluoro-6-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)tetradec-1-ynyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / 30 h / 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; caesium carbonate / ethanol; toluene / 24 h / 73 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; caesium carbonate; diisopropylamine; In ethanol; toluene; 1: Sonogashira coupling / 2: Suzuki coupling;
DOI:10.1021/ic201092s