BOC-VAL-NHNH2

Base Information

• Chemical Name: BOC-VAL-NHNH2
• CAS No.: 72039-28-2
• Molecular Formula: C10H21N3O3
• Molecular Weight: 231.29
• Mol file: 72039-28-2.mol

Synonyms:BOC-VAL-NHNH2;N-ALPHA-T-BUTOXYCARBONYL-L-VALINE HYDRAZIDE;tert-Butyl [(1S)-1-(hydrazinocarbonyl)-2-methylpropyl]carbamate

Chemical Property of BOC-VAL-NHNH2

Chemical Property:

• PSA: 93.45000
• LogP: 2.00770

Purity/Quality:

98% ^*data from raw suppliers

tert-Butyl[(1S)-1-(Hydrazinocarbonyl)-2-methylpropyl]carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-VAL-NHNH2

There total 3 articles about BOC-VAL-NHNH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butoxycarbonyl-L-valine methyl ester (58561-04-9) → tert-butyl [(2S)-1-hydrazino-3-methyl-1-oxobutane-2-yl]carbamate (72039-28-2)

Guidance literature:

With hydrazine hydrate;

Reference yield:

Boc-Val-O-COOEt (98807-40-0) → tert-butyl [(2S)-1-hydrazino-3-methyl-1-oxobutane-2-yl]carbamate (72039-28-2)

Guidance literature:

With hydrazine; In tetrahydrofuran; methanol; at 0 - 20 ℃;

DOI:10.2174/138620710791054303

Reference yield:

→ tert-butyl [(2S)-1-hydrazino-3-methyl-1-oxobutane-2-yl]carbamate (72039-28-2)

Guidance literature:

With hydrazine hydrate; In methanol; at 80 ℃; for 6h;

upstream raw materials:

N-tert-butoxycarbonyl-L-valine methyl ester

Boc-Val-O-COOEt

Downstream raw materials:

C₁₇H₂₆N₄O₃S

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