L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester

Base Information

Chemical Name:L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester
CAS No.:128972-27-0
Molecular Formula:C26H34N2O6
Molecular Weight:470.566
Hs Code.:

Synonyms:L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester

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Chemical Property of L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester

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Technology Process of L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester

There total 3 articles about L-Lysine, N6-[(1,1-diMethylethoxy)carbonyl]-N2-[(phenylMethoxy)carbonyl]-, phenylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.7%

: 2389-60-8
Z-Lys(Boc)-OH

: 100-39-0
benzyl bromide

: 128972-27-0
Nα-carbobenzoxy-Nε-tert-butoxycarbonyl-2,6-diaminohexanoyl benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1002/chem.200305389

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 128972-27-0
Nα-carbobenzoxy-Nε-tert-butoxycarbonyl-2,6-diaminohexanoyl benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Et₃N; aq. NaOH / methanol / 24 h / 20 °C

2: 66 percent / Et₃N / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.10.061

Reference yield:

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 128972-27-0
Nα-carbobenzoxy-Nε-tert-butoxycarbonyl-2,6-diaminohexanoyl benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Et₃N; aq. NaOH / methanol / 24 h / 20 °C

2: 66 percent / Et₃N / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.10.061