3,6-Dimethyl-1-benzofuran-2-carbaldehyde

Base Information

Chemical Name:3,6-Dimethyl-1-benzofuran-2-carbaldehyde
CAS No.:16820-39-6
Molecular Formula:C11H10O2
Molecular Weight:174.2
Hs Code.:2932999099
DSSTox Substance ID:DTXSID30406076
Wikidata:Q82210945
Mol file:16820-39-6.mol

Synonyms:16820-39-6;3,6-dimethyl-1-benzofuran-2-carbaldehyde;3,6-Dimethyl-benzofuran-2-carbaldehyde;3,6-Dimethylbenzofuran-2-carbaldehyde;3,6-dimethylbenzo[b]furan-2-carbaldehyde;SCHEMBL14809632;DTXSID30406076;STL282492;AKOS000267934;BB 0262281;CS-0324215

Suppliers and Price of 3,6-Dimethyl-1-benzofuran-2-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,6-Dimethyl-benzofuran-2-carbaldehyde
100mg
$ 220.00

Matrix Scientific
3,6-Dimethyl-benzofuran-2-carbaldehyde
1g
$ 308.00

Matrix Scientific
3,6-Dimethyl-benzofuran-2-carbaldehyde
500mg
$ 200.00

American Custom Chemicals Corporation
3,6-DIMETHYL-BENZOFURAN-2-CARBALDEHYDE 95.00%
500MG
$ 796.95

AK Scientific
3,6-Dimethyl-benzofuran-2-carbaldehyde
1g
$ 465.00

Total 6 raw suppliers

Chemical Property of 3,6-Dimethyl-1-benzofuran-2-carbaldehyde

Chemical Property:

Melting Point:76-78 °C(Solv: methanol, 80% (67-56-1))
Boiling Point:295.0±35.0 °C(Predicted)
PSA：30.21000
Density:1.157±0.06 g/cm3(Predicted)
LogP:2.86210
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:174.068079557
Heavy Atom Count:13
Complexity:202

Purity/Quality:

98%min ^*data from raw suppliers

3,6-Dimethyl-benzofuran-2-carbaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C(=C(O2)C=O)C

Technology Process of 3,6-Dimethyl-1-benzofuran-2-carbaldehyde

There total 10 articles about 3,6-Dimethyl-1-benzofuran-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24410-50-2
3,6-dimethylbenzofuran

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 16820-39-6
3,6-dimethyl-1-benzofuran-2-carbaldehyde

Guidance literature:: 3,6-dimethylbenzofuran; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 ℃; for 4h;
DOI:10.1016/j.tetlet.2019.03.037

Reference yield:

: 16820-37-4
6-methyl-3-methylcoumarilic acid

: 16820-39-6
3,6-dimethyl-1-benzofuran-2-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅

2: Pd-C

With phosphorus pentachloride; palladium on activated charcoal;

Reference yield:

: 16820-36-3
3,6-dimethyl-benzofuran-2-carboxylic acid ethyl ester

: 16820-39-6
3,6-dimethyl-1-benzofuran-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KOH

2: PCl₅

3: Pd-C

With potassium hydroxide; phosphorus pentachloride; palladium on activated charcoal;