MPEG16-NH2

Base Information

• Chemical Name: MPEG16-NH2
• CAS No.: 907577-50-8
• Molecular Formula: C33H69NO16
• Molecular Weight: 735.9
• Mol file: 907577-50-8.mol

Synonyms:MPEG16-NH2;mPEG16-NH2

Chemical Property of MPEG16-NH2

Chemical Property:

• PSA: 173.70000
• LogP: 0.54080

Purity/Quality:

99.3% ^*data from raw suppliers

mPEG16-NH2 min.97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of MPEG16-NH2

There total 3 articles about MPEG16-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

azidohexadecaethylene glycol methyl ether → deoxyaminohexadecaethylene glycol methyl ether (907577-50-8) + C31H65NO15

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; for 20h;

DOI:10.1002/anie.200804623

Reference yield:

azidohexadecaethylene glycol methyl ether → deoxyaminohexadecaethylene glycol methyl ether (907577-50-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃;

DOI:10.1002/anie.201813125

Reference yield:

hexadecylethylene glycol monomethylether (133604-58-7) → deoxyaminohexadecaethylene glycol methyl ether (907577-50-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine; methanesulfonyl chloride / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

1.2: 144 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

With palladium 10% on activated carbon; hydrogen; methanesulfonyl chloride; triethylamine; In dichloromethane; ethyl acetate;

DOI:10.1002/anie.201813125

upstream raw materials:

hexadecylethylene glycol monomethylether