4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL

Base Information

Chemical Name:4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL
CAS No.:41032-95-5
Molecular Formula:C22H22O3
Molecular Weight:334.41
Hs Code.:2909309090
Mol file:41032-95-5.mol

Synonyms:4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL

Suppliers and Price of 4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4,4'-DIMETHOXY-4'-METHYLTRITYL ALCOHOL 95.00%
0.5G
$ 1127.50

AHH
4,4-Dimethoxy-4-methyltritylalcohol 95%
5g
$ 500.00

Total 5 raw suppliers

Chemical Property of 4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL

Chemical Property:

PSA：38.69000
LogP:4.29640

Purity/Quality:

98%min ^*data from raw suppliers

4,4'-DIMETHOXY-4'-METHYLTRITYL ALCOHOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL

There total 2 articles about 4,4'-DIMETHOXY-4''-METHYLTRITYL ALCOHOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 99-75-2
4-methyl-benzoic acid methyl ester

: 104-92-7
1-bromo-4-methoxy-benzene

: 41032-95-5
4,4'-dimethoxy-4''-methyltriphenylmethanol

Guidance literature:: 1-bromo-4-methoxy-benzene; With magnesium; In tetrahydrofuran; at 20 ℃;

4-methyl-benzoic acid methyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

: 41032-95-5
4,4'-dimethoxy-4''-methyltriphenylmethanol

Guidance literature:: 4,4'-Dimethoxybenzophenon, 4-Tolylmagnesiumbromid;
DOI:10.1002/macp.1973.021640105

Reference yield:

: 41032-95-5
4,4'-dimethoxy-4''-methyltriphenylmethanol

: 541541-07-5
4-[[2-(tert-butyldimethylsilyloxy)ethyl]sulfonylmethyl]-4',4''-dimethoxytrityl 1-methylethyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: acetyl chloride / 1 h / Heating

2: pyridine / 0 °C

3: N-bromosuccinimide; N,N'-azobisisobutyronitrile / CCl₄ / 0.33 h / Heating

4: 24 g / N-ethyldiisopropylamine / dimethylformamide / 3 h / 20 °C

5: 62 percent / m-chloroperbenzoic acid; sodium bicarbonate / CH₂Cl₂ / 0.17 h / 0 °C

6: 97 percent / imidazole / dimethylformamide / 1 h / 20 °C

With pyridine; 1H-imidazole; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;