N,N-Dimethylthiocarbamic acid O-cyclohexyl ester

Base Information

• Chemical Name: N,N-Dimethylthiocarbamic acid O-cyclohexyl ester
• CAS No.: 21299-34-3
• Molecular Formula: C9H17NOS
• Molecular Weight: 187.306
• Mol file: 21299-34-3.mol

Synonyms:N,N-Dimethylthiocarbamic acid O-cyclohexyl ester

Chemical Property of N,N-Dimethylthiocarbamic acid O-cyclohexyl ester

Chemical Property:

• PSA: 44.56000
• LogP: 2.18220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-Dimethylthiocarbamic acid O-cyclohexyl ester

There total 2 articles about N,N-Dimethylthiocarbamic acid O-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-Dimethylthiocarbamoyl chloride (16420-13-6) + cyclohexanol (108-93-0) → dimethyl-thiocarbamic acid O-cyclohexyl ester (21299-34-3)

Guidance literature:

Multistep reaction; (i) NaH, DMF, (ii) /BRN= 635823/;

DOI:10.1021/jo01263a083

Reference yield:

→ dimethyl-thiocarbamic acid O-cyclohexyl ester (21299-34-3)

Guidance literature:

/BRN= 3239105/;

Reference yield:

dimethyl-thiocarbamic acid O-cyclohexyl ester (21299-34-3) + bromoacetic acid (79-08-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 1-bromocyclohexane (108-85-0) + dimethylcarbamoylsulfanyl-acetic acid (29596-84-7)

Guidance literature:

upstream raw materials:

N,N-Dimethylthiocarbamoyl chloride

cyclohexanol

Downstream raw materials:

S-benzy-N,N-dimethyl thiocarbamate

1-bromocyclohexane

dimethylcarbamoylsulfanyl-acetic acid