Apadtg

Base Information

Chemical Name:Apadtg
CAS No.:3459-29-8
Molecular Formula:C14H20N2O6
Molecular Weight:312.3184
Hs Code.:
DSSTox Substance ID:DTXSID20956095
Mol file:3459-29-8.mol

Synonyms:4-aminophenyl-2-acetamido-2-deoxyglucoside;APADTG;p-aminophenyl-2-acetamido-2-deoxy-beta-D-glucoside

Suppliers and Price of Apadtg

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Apadtg

Chemical Property:

Vapor Pressure:6.63E-19mmHg at 25°C
Boiling Point:670.7°Cat760mmHg
Flash Point:359.4°C
Density:1.43g/cm³
XLogP3:-1.1
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:312.13213636
Heavy Atom Count:22
Complexity:374

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NC1C(C(C(OC1OC2=CC=C(C=C2)N)CO)O)O
Isomeric SMILES:CC(=O)N[C@@H]1[C@H]([C@@H]([C@H](OC1OC2=CC=C(C=C2)N)CO)O)O

Technology Process of Apadtg

There total 9 articles about Apadtg which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3459-18-5,50645-66-4
4-nitrophenyl N-acetyl-β-D-glucosaminide

: 14419-59-1,3459-29-8
4-aminophenyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 0.166667h; Heating;

Reference yield: 61.8%

: 65907-85-9
p-aminophenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-β-D-glucopyranoside

: 14419-59-1,3459-29-8
4-aminophenyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; chloroform; acetonitrile; for 1h; Ambient temperature;
DOI:10.1248/cpb.43.266

Reference yield:

: 13089-27-5,13089-23-1
p-nitrophenyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranoside

: 14419-59-1,3459-29-8
4-aminophenyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91.3 percent / H₂ / 10percent Pd/C / ethanol; dioxane / 3 h / 760 Torr / Ambient temperature

2: 61.8 percent / 28percent NaOMe / methanol; acetonitrile; CHCl₃ / 1 h / Ambient temperature

With hydrogen; sodium methylate; palladium on activated charcoal; In 1,4-dioxane; methanol; ethanol; chloroform; acetonitrile;
DOI:10.1248/cpb.43.266